A comparison of pyrrolidide and picolinyl ester derivatives for the identification of fatty acids in natural samples by gas chromatography-mass spectrometry.

Abstract:

:The pyrrolidide and picolinyl ester derivatives of the fatty acids in two natural lipid samples rich in unsaturated fatty acids, pig testis lipids and cod liver oil were satisfactorily resolved on capillary columns of fused silica coated with stationary phases of varying polarity. The picolinyl esters, in particular, when subjected to gas chromatography-mass spectrometry on a column containing a cross-linked methyl silicone, gave distinctive mass spectra, which could be interpreted in terms of both the numbers and positions of the double bonds.

journal_name

Lipids

journal_title

Lipids

authors

Christie WW,Brechany EY,Johnson SB,Holman RT

doi

10.1007/BF02537217

subject

Has Abstract

pub_date

1986-10-01 00:00:00

pages

657-61

issue

10

eissn

0024-4201

issn

1558-9307

journal_volume

21

pub_type

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