Sono-chemical preparation of cellulose nanocrystals from lignocellulose derived materials.

Abstract:

:This study examined the production of cellulose nanocrystals from microcrystalline wood cellulose, Avicel and recycled pulp of wood pulp using sono-chemical-assisted hydrolysis. Two hydrolysis systems: deionized water and maleic acid were evaluated. In deionized water, Avicel produced cellulose nanocrystals with average diameter of 21+/-5 nm (minimum 15 nm and maximum 32 nm). Cellulose nanocrystals from recycled pulp were not distinctively spherical and had an average diameter of 23+/-4 nm (minimum 14 nm and maximum 32 nm). Maleic acid (50 mM) sono-chemical assisted hydrolysis of Avicel at 15 degrees C and 90% power output for 9 min produced cellulose nanocrystals which were cylindrical in shape and were of dimensions, length 65+/-19 nm and width 15 nm.

journal_name

Bioresour Technol

journal_title

Bioresource technology

authors

Filson PB,Dawson-Andoh BE

doi

10.1016/j.biortech.2008.09.062

subject

Has Abstract

pub_date

2009-04-01 00:00:00

pages

2259-64

issue

7

eissn

0960-8524

issn

1873-2976

pii

S0960-8524(08)00859-6

journal_volume

100

pub_type

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