Abstract：
:The forensic toxicology community has recognized flunitrazepam and its metabolite (7-aminoflunitrazepam) as compounds of concern for several years. In this procedure, the analytes were extracted from whole blood and urine onto single mode solid phase cartridges (butyl) using nitrazepam as an internal standard. The columns were washed with distilled water and hexane. All three compounds were eluted from the sorbent using an ethyl acetate-methanol solvent mixture. After collection and evaporation of the solvent, the residue was dissolved in A, 0.1% (v/v) aqueous trifluoroacetic acid for HPLC-PDA analysis or B, ethyl acetate for derivatization with pentafluoropropionic anhydride (PFPA) for analysis by gas chromatography-mass spectrometry (selected ion monitoring, SIM). A limit of quantitation for this method using HPLC-PDA was found to be 5 and 1.0 ng mL(-1) by SIM.
journal_name
Forensic Sci Intjournal_title
Forensic science internationalauthors
Hackett J,Elian AAdoi
10.1016/j.forsciint.2005.03.019keywords:
subject
Has Abstractpub_date
2006-03-10 00:00:00pages
156-62issue
2-3eissn
0379-0738issn
1872-6283pii
S0379-0738(05)00190-8journal_volume
157pub_type
杂志文章abstract：:Investigating crimes against children, specifically sexual solicitations, are complicated because not all offenders are contact-driven, meaning they want to meet the minor for sex in the physical world; instead, some offenders are fantasy-driven, in that they are more interested in cybersex and role-play. In addition,...
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journal_title：Forensic science international
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journal_title：Forensic science international
pub_type： 杂志文章
doi：10.1016/s0379-0738(03)00110-5
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doi：10.1016/j.forsciint.2004.09.041
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journal_title：Forensic science international
pub_type： 杂志文章
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更新日期：1992-10-01 00:00:00
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journal_title：Forensic science international
pub_type： 杂志文章
doi：10.1016/j.forsciint.2017.04.005
更新日期：2017-08-01 00:00:00
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pub_type： 杂志文章
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更新日期：1994-12-16 00:00:00
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journal_title：Forensic science international
pub_type： 杂志文章
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journal_title：Forensic science international
pub_type： 历史文章,杂志文章
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更新日期：1999-01-25 00:00:00
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journal_title：Forensic science international
pub_type： 杂志文章
doi：10.1016/j.forsciint.2007.08.007
更新日期：2008-05-02 00:00:00
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journal_title：Forensic science international
pub_type： 杂志文章
doi：10.1016/0379-0738(93)90053-d
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journal_title：Forensic science international
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更新日期：2017-12-01 00:00:00
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journal_title：Forensic science international
pub_type： 杂志文章
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journal_title：Forensic science international
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journal_title：Forensic science international
pub_type： 杂志文章
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更新日期：2006-08-10 00:00:00
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更新日期：2011-01-30 00:00:00
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journal_title：Forensic science international
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更新日期：2013-02-10 00:00:00
abstract：:The amplification of the STR DYS391, using the primers described in the Genome Data Base (GDB: G00-365-251), shows not only an additional band to the Y-specific one in males with a size range of 26 bp less than those of DYS391 locus alleles, but also a polymorphic pattern in females in the same size range as the addit...
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更新日期：2000-07-24 00:00:00
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pub_type： 杂志文章
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更新日期：1994-05-25 00:00:00
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journal_title：Forensic science international
pub_type： 杂志文章
doi：10.1016/0379-0738(82)90150-5
更新日期：1982-01-01 00:00:00
abstract：:Forensic anthropology makes an important contribution to human identification and assessment of the causes and mechanisms of death and body disposal in criminal and civil investigations, including those related to atrocity, disaster and trafficking victim identification. The methods used are comparative, relying on as...
journal_title：Forensic science international
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更新日期：2017-10-01 00:00:00
