Abstract：
:Four commercial hydroxyapatites (both natural and synthetic) were tested to assess transformations of the chemical and crystalline structure following variation of temperature from 20 to 1600 degrees C. The thermal behaviour of hydroxyapatite is relevant for biomedical applications such as plasma spraying of metallic implants. Thermogravimetric analysis showed a weight loss from each hydroxyapatite specimen, due to a release of structural H2O molecules; all the specimens up to 1300 degrees C were made of crystalline hydroxyapatite, determined by X-ray diffraction; at 1470 degrees C they were made of both hydroxyapatite and calcium phosphate, but at 1570 degrees C of calcium phosphate exclusively. The diffractograms of the hydroxyapatite coatings showed the same peaks as the original powders, so at the chosen plasma-spray procedure level no new phases were formed. The peak height was nevertheless lower in the plasma-sprayed hydroxyapatites for all interplanar spacing values, which indicated a lower degree of crystallinity, associated with a random structure derived from an alteration to the original crystalline network.
journal_name
Biomaterialsjournal_title
Biomaterialsauthors
Locardi B,Pazzaglia UE,Gabbi C,Profilo Bdoi
10.1016/0142-9612(93)90146-ssubject
Has Abstractpub_date
1993-05-01 00:00:00pages
437-41issue
6eissn
0142-9612issn
1878-5905pii
0142-9612(93)90146-Sjournal_volume
14pub_type
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