Separation and determination of coumarins in the root bark of three citrus plants by micellar electrokinetic capillary chromatography.

Abstract:

:A micellar electrokinetic capillary chromatography (MEKC) method for the determination of xanthyletin and xanthoxyletin in the roots bark of three Citrus plants was developed for the first time. The electrophoresis buffer was 10 mmol/L sodium borate containing 50 mmol/L sodium dodecyl sulfate, 20% (v/v) acetonitrile and 10 % (v/v) methanol (pH 9.8). The correlation coefficients of the calibration curves for xanthyletin and xanthoxyletin are 0.9993 and 0.9999, respectively, over the concentration ranges (16.0-800.0 mg/L; 8.0-400.0 mg/L).

journal_name

Planta Med

journal_title

Planta medica

authors

Wang SF,Ju Y,Chen XG,Hu ZD

doi

10.1055/s-2003-39697

subject

Has Abstract

pub_date

2003-05-01 00:00:00

pages

483-6

issue

5

eissn

0032-0943

issn

1439-0221

journal_volume

69

pub_type

信件
  • Formation of Digitalis lanata Clone Lines by Shoot Tip Culture.

    abstract::Propagation of DIGITALIS LANATA by shoot tip culture made possible (a) the rapid multiplication of elite plants with the formation of plant clones and (b) the long-term cultivation of these plants which under normal growth conditions would die at the end of the second vegetation period. Optimum conditions were establi...

    journal_title:Planta medica

    pub_type: 杂志文章

    doi:10.1055/s-2006-960883

    authors: Diettrich B,Mertinat H,Luckner M

    更新日期:1990-02-01 00:00:00

  • (3R,6R)-4-methyl-6-(1-methylethyl)-3-phenylmethyl-perhydro-1,4-oxazine-2,5-dione: an apoptosis-inducer from the fruiting bodies of Isaria japonica.

    abstract::(3R,6R)-4-methyl-6-(1-methylethyl)-3-phenylmethylperhydro-1,4-oxazine-2,5-dione (1) was isolated from the fruiting bodies of Isaria japonica as an apoptosis-inducing agent. The complete structural assignment of the compound was accomplished on the basis of spectroscopic methods and chemical transformations. Compound 1...

    journal_title:Planta medica

    pub_type: 杂志文章

    doi:10.1055/s-2002-26744

    authors: Oh H,Kim T,Oh GS,Pae HO,Hong KH,Chai KY,Kwon TO,Chung HT,Lee HS

    更新日期:2002-04-01 00:00:00

  • [Plants from new caledonia: alkaloids of stem-bark of Hernandia cordigera].

    abstract::The alkaloidal content of of the stem barks of Hernandia cordigera has been studied and compared to that of other Hernandia species. Main alkaloids are phenolic aporphines. ...

    journal_title:Planta medica

    pub_type: 杂志文章

    doi:10.1055/s-2007-971545

    authors: Lavault M,Debray MM,Bruneton J

    更新日期:1981-05-01 00:00:00

  • Sarothrin from Alkanna orientalis is an antimicrobial agent and efflux pump inhibitor.

    abstract::An Alkanna orientalis leaf and flower extract inhibited the growth of Staphylococcus aureus, a pathogen that causes an estimated 478 000 hospitalizations in the US annually. Bioassay-guided fractionation of A. orientalis resulted in isolation of the flavonoid sarothrin (5,7,4'-trihydroxy-3,6,8-trimethoxyflavone), whic...

    journal_title:Planta medica

    pub_type: 杂志文章

    doi:10.1055/s-0032-1328259

    authors: Bame JR,Graf TN,Junio HA,Bussey RO 3rd,Jarmusch SA,El-Elimat T,Falkinham JO 3rd,Oberlies NH,Cech RA,Cech NB

    更新日期:2013-03-01 00:00:00

  • [A comparative study of the effects of selection and environmental factors on alkaloid accumulation in strains of Choisya ternata].

    abstract::The accumulation of two dihydrofuroquinoline alkaloids has been studied in seventeen strains of Choisya ternata (Rutaceae) initiated from the same tree. The contents of platydesminium and balfourodinium vary in heavy proportions. The effect of some factors (age of the culture, NAA or glucose concentrations of the medi...

    journal_title:Planta medica

    pub_type: 杂志文章

    doi:10.1055/s-2007-971221

    authors: Gras M,Crèche J,Chénieux JC,Rideau M

    更新日期:1982-12-01 00:00:00

  • Re-introduction of kava (Piper methysticum) to the EU: is there a way forward?

    abstract::Kava (Piper methysticum) is an effective anxiolytic that has been withdrawn from various consumer markets in European countries due to concerns over its hepatotoxicity. It is plausible that the reported hepatotoxicity may be due in part to plant substitution, or an incorrect cultivar, or plant parts being used (such a...

    journal_title:Planta medica

    pub_type: 杂志文章

    doi:10.1055/s-0030-1250290

    authors: Sarris J,Teschke R,Stough C,Scholey A,Schweitzer I

    更新日期:2011-01-01 00:00:00

  • Possible active components of tan-shen (Salvia miltiorrhiza) for protection of the myocardium against ischemia-induced derangements.

    abstract::Extract of Tan-Shen (Salvia miltiorrhiza, Labiatae), a Chinese traditional crude drug, was reported to show beneficial activity for heart disease. Chemical examination on the extract was performed on the basis of screening for protective action on the ischemic myocardium. Isolated hearts were subjected to hypoxic perf...

    journal_title:Planta medica

    pub_type: 杂志文章

    doi:10.1055/s-2006-961824

    authors: Yagi A,Fujimoto K,Tanonaka K,Hirai K,Takeo S

    更新日期:1989-02-01 00:00:00

  • Depsides from the petals of Papaver rhoeas.

    abstract::Two new depsides as well as the known p-hydroxybenzoic acid and its methyl ester, protocatechuic acid, 2-(4-hydroxyphenyl)-ethanol, 2-(3,4-dihydroxyphenyl)-ethanol and the flavonoids kaempferol, quercetin, luteolin and hypolaetin and the glycosides 3- O-beta- D-glucopyranosylquercetin (isoquercitrine), 3- O-beta- D-gl...

    journal_title:Planta medica

    pub_type: 杂志文章

    doi:10.1055/s-2004-818956

    authors: Hillenbrand M,Zapp J,Becker H

    更新日期:2004-04-01 00:00:00

  • Isoflavonoids from Pueraria mirifica and their estrogenic activity.

    abstract::Nine isoflavonoids including a new pterocarpene, puemiricarpene, were isolated from the tuberous root of Pueraria mirifica (Leguminosae). The structure of puemiricarpene was determined by spectroscopic means. Estrogenic activity of the isolated isoflavonoids was tested using MCF-7 human breast cancer cells. Moderate a...

    journal_title:Planta medica

    pub_type: 信件

    doi:10.1055/s-2000-8603

    authors: Chansakaow S,Ishikawa T,Sekine K,Okada M,Higuchi Y,Kudo M,Chaichantipyuth C

    更新日期:2000-08-01 00:00:00

  • Interactions of viscotoxins with vesicles of genuine plant membranes.

    abstract::Extracts of Viscum album L. produced by a specific homogenization procedure contain viscotoxins (VT) and liposome-like membrane vesicles, formed from cellular membranes. Interactions between these membrane structures and viscotoxins are characterized in this work. Binding properties of viscotoxins with mistletoe extra...

    journal_title:Planta medica

    pub_type: 杂志文章

    doi:10.1055/s-2008-1034282

    authors: Winkler K,Jäger S,Leneweit G,Schubert R

    更新日期:2008-02-01 00:00:00

  • [Barbatoside, a new Iridoid glucoside from Penstemon barbatus].

    abstract::From leaves of Penstemon barbatus Nutt. a new iridoid glucoside has been isolated. The structure was established mainly by spectroscopic methods ( (1)H-NMR, (13)C-NMR, IR, MS). ...

    journal_title:Planta medica

    pub_type: 杂志文章

    doi:10.1055/s-2007-971261

    authors: Junior P

    更新日期:1982-06-01 00:00:00

  • Radical scavengers from the entomogenous deuteromycete Beauveria amorpha.

    abstract::The culture medium of Beauveria amorpha Hohn. exhibited strong radical scavenging properties. Activity-directed fractionation assisted by a radical scavenging assay on TLC afforded two active compounds which were identified as 6-methyl-2,4-dihydroxyphenyl 4-O-methyl-beta-D-glucopyranoside (1) and (-)-terredionol (2). ...

    journal_title:Planta medica

    pub_type: 信件

    doi:10.1055/s-2002-19868

    authors: Hu F,Schmidt K,Stoyanova S,Zengzhi L,Gräfe U,Hamburger M

    更新日期:2002-01-01 00:00:00

  • Leaf alkaloid contents of Tabernaemontana pachysiphon as influenced by endogenous and environmental factors in the natural habitat.

    abstract::Indole alkaloid contents were investigated in leaves of Tabernaemontana pachysiphon (Apocynaceae) trees in the natural habitat, Shimba Hills National Reserve, Kenya. The contents of the major alkaloids apparicine, tubotaiwine, tubotaiwine- N-oxide, and isovoacangine varied with site, leaf age, leaf growth form, positi...

    journal_title:Planta medica

    pub_type: 杂志文章

    doi:10.1055/s-2006-957393

    authors: Höft M,Verpoorte R,Beck E

    更新日期:1998-03-01 00:00:00

  • Absolute/relative bioavailability and metabolism of dodeca-2E,4E,8Z,10E/Z-tetraenoic acid isobutylamides (tetraenes) after intravenous and oral single doses to rats.

    abstract::The present study assessed the absolute and relative bioavailabilities of dodeca-2 E,4 E,8 Z,10 E/ Z-tetraenoic acid isobutylamides (tetraenes), the main bioactive constituents in Echinacea, administered as pure compounds or in the form of an Echinacea purpurea root extract preparation. Tetraenes were administered ora...

    journal_title:Planta medica

    pub_type: 杂志文章

    doi:10.1055/s-0030-1271120

    authors: Ardjomand-Woelkart K,Kollroser M,Magnes C,Sinner F,Frye RF,Derendorf H,Bauer R,Butterweck V

    更新日期:2011-11-01 00:00:00

  • Antitrypanosomal isothiocyanate and thiocarbamate glycosides from Moringa peregrina.

    abstract::O-Methyl (1), O-ethyl (2), and O-butyl (3) 4-[(α-L-rhamnosyloxy) benzyl] thiocarbamate (E), along with 4-(α-L-rhamnosyloxy) benzyl isothiocyanate (4) have been isolated from the aerial parts of Moringa peregrina. The compounds were tested for in vitro activity against Trypanosoma brucei rhodesiense and cytotoxicity in...

    journal_title:Planta medica

    pub_type: 杂志文章

    doi:10.1055/s-0033-1351102

    authors: Ayyari M,Salehi P,Ebrahimi SN,Zimmermann S,Portmann L,Krauth-Siegel RL,Kaiser M,Brun R,Rezadoost H,Rezazadeh S,Hamburger M

    更新日期:2014-01-01 00:00:00

  • [On the gas-chromatographical determination of the pyrrolizidine alkaloids of some Senecio-species].

    abstract::A gas-chromatographical method is described on which seven pyrrolizidine alkaloids (Fuchsisenecionine, Senecionine, Senecivernine, Senkirkine, Retrorsine, O (7)-Angelylheliotridine and Heliotrine) are determinated in a qualitative way and their ratio of concentration in Senecio fuchsii, vernalis, inaequidens and ovire...

    journal_title:Planta medica

    pub_type: 杂志文章

    doi:10.1055/s-2007-971688

    authors: Wiedenfeld H,Pastewka U,Stengl P,Röder E

    更新日期:1981-02-01 00:00:00

  • Inhibition of prostate cancer (LNCaP) cell proliferation by volatile components from Nagami kumquats.

    abstract::Fresh Nagami kumquats (Fortunella margarita) were subjected to hydrodistillation using a Clevenger-type apparatus to obtain volatile oil. The chemical composition of the volatile oil was analyzed by GC-MS using Rtx-5 Sil MS and DB Wax columns. A total of 25 volatile compounds were identified by mass spectra, retention...

    journal_title:Planta medica

    pub_type: 杂志文章

    doi:10.1055/s-0031-1298619

    authors: Jayaprakasha GK,Murthy KN,Demarais R,Patil BS

    更新日期:2012-06-01 00:00:00

  • Inhibitors of nitric oxide synthesis and TNF-alpha expression from Magnolia obovata in activated macrophages.

    abstract::Nitric oxide (NO) and tumor necrosis factor-alpha (TNF-alpha) are the major mediators produced in activated macrophages which contribute to the circulatory failure associated with septic shock. An activity-guided fractionation of an MeOH extract of stem bark of Magnolia obovata afforded two inhibitors of NO production...

    journal_title:Planta medica

    pub_type: 信件

    doi:10.1055/s-2000-8592

    authors: Son HJ,Lee HJ,Yun-Choi HS,Ryu JH

    更新日期:2000-06-01 00:00:00

  • Trypanocidal activity of a new diterpene from Casearia sylvestris var. lingua.

    abstract::Bioassay-guided fractionation of the hexanic root bark extract of Casearia sylvestris var. lingua led to the isolation of a new clerodane diterpene, whose structure was elucidated as rel-(2 S,5 R,6 R,8 S,9 S,10 R,18 S,19 R)-19-acetoxy-18,19-epoxy-6-hydroxy-18-butanoyloxy-2-(2-methylbutanoyloxy)cleroda-3,13(16), 14-tri...

    journal_title:Planta medica

    pub_type: 杂志文章

    doi:10.1055/s-2004-832655

    authors: Espindola LS,Vasconcelos Júnior JR,de Mesquita ML,Marquié P,de Paula JE,Mambu L,Santana JM

    更新日期:2004-11-01 00:00:00

  • Prediction of the Passive Intestinal Absorption of Medicinal Plant Extract Constituents with the Parallel Artificial Membrane Permeability Assay (PAMPA).

    abstract::At the early drug discovery stage, the high-throughput parallel artificial membrane permeability assay is one of the most frequently used in vitro models to predict transcellular passive absorption. While thousands of new chemical entities have been screened with the parallel artificial membrane permeability assay, in...

    journal_title:Planta medica

    pub_type: 杂志文章

    doi:10.1055/s-0042-101247

    authors: Petit C,Bujard A,Skalicka-Woźniak K,Cretton S,Houriet J,Christen P,Carrupt PA,Wolfender JL

    更新日期:2016-03-01 00:00:00

  • Fast and Green - CO2 Based Extraction, Isolation, and Quantification of Phenolic Styrax Constituents.

    abstract::In this study the first supercritical fluid based protocol for the extraction, analysis, and isolation of six polar compounds, i.e., o-vanillin (1), styracin (2), vanillin (3), trans-cinnamic acid (4), vanillic acid (5), and shikimic acid (6), was developed. First, eight styrax resin products (R1-R8) obtained from var...

    journal_title:Planta medica

    pub_type: 杂志文章

    doi:10.1055/s-0043-105499

    authors: Scheuba J,Wronski VK,Rollinger JM,Grienke U

    更新日期:2017-08-01 00:00:00

  • Antiplatelet aggregation principles from Ephemerantha lonchophylla.

    abstract::Bioactivity-directed separation led to the identification of four compounds, viz. denbinobin (1), 3,7-dihydroxy-2,4-dimethoxyphenanthrene (2), 3-methylgigantol (3), and erianthridin (4) from the ethanolic extract of Ephemerantha lonchophylla. Antiplatelet tests were carried out using 4 different aggregation inducers, ...

    journal_title:Planta medica

    pub_type: 信件

    doi:10.1055/s-2000-8553

    authors: Chen CC,Huang YL,Teng CM

    更新日期:2000-05-01 00:00:00

  • Antibacterial properties of phenolic triterpenoids against Staphylococcus epidermidis.

    abstract::Two phenolic triterpenoids, pristimerol (30 µg/mL) and 8- EPI-6-deoxoblepharodol (20 µg/mL), obtained by catalytic reduction of pristimerin, exhibited bacteriostatic action against Staphylococcus epidermidis. This activity was not dependent on the inoculum size and the growth phase although it showed a stronger effect...

    journal_title:Planta medica

    pub_type: 杂志文章

    doi:10.1055/s-0030-1250500

    authors: López MR,de León L,Moujir L

    更新日期:2011-05-01 00:00:00

  • Seasonal variation of phenolic constituents and medicinal activities of Northern Labrador tea, Rhododendron tomentosum ssp. subarcticum, an Inuit and cree First Nations traditional medicine.

    abstract::Northern Labrador tea, Rhododendron tomentosum ssp. subarcticum, is one of the most commonly used medicinal plants by Inuit and other First Nations peoples of Canada. The phenolic profile and seasonal variation of this commonly used medicinal plant remains largely unknown. To assess optimal harvesting time, R. tomento...

    journal_title:Planta medica

    pub_type: 杂志文章

    doi:10.1055/s-0030-1270968

    authors: Black P,Saleem A,Dunford A,Guerrero-Analco J,Walshe-Roussel B,Haddad P,Cuerrier A,Arnason JT

    更新日期:2011-09-01 00:00:00

  • Induction of cytochrome P450s by rutaecarpine and metabolism of rutaecarpine by cytochrome P450s.

    abstract::Rutaecarpine is an alkaloid originally isolated from the unripe fruit of Evodia rutaecarpa. Recently, rutaecarpine has been characterized to have an anti-inflammatory activity through cyclooxygenase-2 inhibition. In the present studies, the effects of rutaecarpine on liver cytochrome P450 s (P450s) and P450 s involved...

    journal_title:Planta medica

    pub_type: 杂志文章

    doi:10.1055/s-2004-827207

    authors: Lee SK,Kim NH,Lee J,Kim DH,Lee ES,Choi HG,Chang HW,Jahng Y,Jeong TC

    更新日期:2004-08-01 00:00:00

  • Aescin Content in Embryogenic Callus and in Embryoids from Leaf Explants of Aesculus hippocastanum.

    abstract::HPLC determinations of the aescin contents in calli and embryoids from leaf explants of AESCULUS HIPPOCASTANUM L. were carried out in order to determine whether it was possible to obtain aescin-forming proliferations IN VITRO. The results indicate that embryogenic calli and embryoids derived from them produce an amoun...

    journal_title:Planta medica

    pub_type: 杂志文章

    doi:10.1055/s-2006-960016

    authors: Profumo P,Caviglia AM,Gastaldo P,Dameri RM

    更新日期:1991-02-01 00:00:00

  • Two New Anthraquinones from the Seeds of Peganum harmala.

    abstract::Two new anthraquinones have been isolated from the seeds of PEGANUM HARMALA Linn and the structures established as 3,6-dihydroxy-8-methoxy-2-methylanthraquinone (peganone; 1) and 8-hydroxy-7-methoxy-2-methylanthraquinone (peganone; 2) by spectral correlations and chemical evidences. ...

    journal_title:Planta medica

    pub_type: 杂志文章

    doi:10.1055/s-2006-962639

    authors: Pitre S,Srivastava SK

    更新日期:1987-02-01 00:00:00

  • Simultaneous determination of the absolute configuration of twelve monosaccharide enantiomers from natural products in a single injection by a UPLC-UV/MS method.

    abstract::In natural product chemistry, it is often crucial to determine sugar composition as well as the absolute configuration of each monosaccharide in glycosides. An ultra-performance liquid chromatography method using both photodiode array (PDA) and mass spectrometry detectors (UPLC-UV/MS) was developed for qualitative ana...

    journal_title:Planta medica

    pub_type: 杂志文章

    doi:10.1055/s-0031-1298432

    authors: Wang YH,Avula B,Fu X,Wang M,Khan IA

    更新日期:2012-05-01 00:00:00

  • An approach to the antiinflammatory activity of borjatriol.

    abstract::The antiinflammatory activity of borjatriol (a diterpenoid isolated from SIDERITIS MUGRONENSIS Borja) was tested using the cotton pellet-granuloma assay. The compound inhibited the granuloma weight and the serum lysozyme activity in a dose-dependently way. The determination of this enzyme has allowed us to distinguish...

    journal_title:Planta medica

    pub_type: 杂志文章

    doi:10.1055/s-2007-969630

    authors: Villar A,Salom R,Alcaraz MJ

    更新日期:1984-02-01 00:00:00

  • Chemical Study on the Alkaloids of Corydalis hsuchowensis.

    abstract::Ten alkaloids were isolated from the bulb of CORYDALIS HSUCHOWENSIS W. Y. Lian nov. ined. Among them nine alkaloids are known, identified as (-)-stylopine ( 1), cheilanthifoline ( 2), (+)-adlumidine ( 3), (+)-bicuculline ( 4), sibiricine ( 5), humosine A ( 6), (+)-bulbocapnine ( 7), (-)-scoulerine ( 8), and protopine ...

    journal_title:Planta medica

    pub_type: 杂志文章

    doi:10.1055/s-2006-960054

    authors: Zhou JY,Tong XJ,Lian WY,Fang QC

    更新日期:1991-04-01 00:00:00