Abstract:
:A quantitative gas chromatographic assay for the determination of phenelzine in plasma or other fluids is presented. A stable derivative is formed by cyclization with acetylacetone, and the derivative is separated, purified, and concentrated by liquid-liquid solvent extraction. Analysis of the extracts is by capillary gas chromatography with nitrogen specific detection. Detection limits of less than 1 ng/mL and CVs of 5% at the 10-ng/mL level are attainable with a 2-mL sample and benzylhydrazine as the internal standard.
journal_name
J Anal Toxicoljournal_title
Journal of analytical toxicologyauthors
Lichtenwalner M,McMullin M,Hardy D,Rieders Fdoi
10.1093/jat/12.2.98subject
Has Abstractpub_date
1988-03-01 00:00:00pages
98-101issue
2eissn
0146-4760issn
1945-2403journal_volume
12pub_type
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