Abstract:
:A C6-carboxylated curdlan (C6-Cc) obtained from 4-acetamido-TEMPO-mediated oxidation of curdlan was used both as a reducing and stabilizing agent for green synthesis of pH-responsive AuNPs, which was carried out by controlling the pH of the C6-Cc solution at a high temperature (100°C). C6-Cc presented a semi-flexible random coil chain in the aqueous medium at pH 5.5 and became more expanded and rigid in alkaline conditions (pH 7.1-12.0), though the primary chemical structure of C6-Cc was virtually unchanged with the pH variation. The AuNPs prepared with C6-Cc at various pHs were characterized by various instrumental measurements. The shapes and sizes of AuNPs were found to be strongly dependent on the pH of the C6-Cc solution. The C6-Cc-decorated AuNPs exhibited a more well-dispersed spherical morphology with smaller particle sizes under alkaline conditions (pH 7.1-12.0). Through this study, a facile, simple, and green method has been demonstrated for preparation of stimuli-sensitive AuNPs using biocompatible polyanionic polysaccharides.
journal_name
Int J Biol Macromoljournal_title
International journal of biological macromoleculesauthors
Qiu WY,Wang K,Wang YY,Ding ZC,Wu LX,Cai WD,Yan JKdoi
10.1016/j.ijbiomac.2017.08.029subject
Has Abstractpub_date
2018-01-01 00:00:00pages
498-506eissn
0141-8130issn
1879-0003pii
S0141-8130(17)32149-9journal_volume
106pub_type
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