Abstract:
:Melamine is a nitrogenous chemical substance used principally as a starting material for the manufacture of synthetic resins. Due to its very high proportion of nitrogen melamine has been added illegitimately to foods and feeds to increase the measured protein content, which determines the value of the product. These issues prompted private as well as governmental laboratories to develop methods for the analysis of melamine in a wide variety of food products and ingredients. Owing to this fact present study is aimed to use single bounce attenuated total reflectance (SB-ATR) Fourier transform infrared spectroscopy (FTIR) method as an effective rapid tool for the detection and quantification of melamine in milk (liquid and powder). Partial least-squares (PLS) models were established for correlating spectral data to melamine concentration with R(2)>0.99, and RMSEC 0.370. Linear calibration curves were obtained over the calibration range of 25-0.0625%. The LOD and LOQ of the method was 0.00025% (2.5 ppm) and 0.0015% (15 ppm) respectively. Proposed SB-ATR-FTIR method requires little or no sample preparation with an assay time of 1-2 min.
journal_name
Food Chemjournal_title
Food chemistryauthors
Jawaid S,Talpur FN,Sherazi ST,Nizamani SM,Khaskheli AAdoi
10.1016/j.foodchem.2013.05.106subject
Has Abstractpub_date
2013-12-01 00:00:00pages
3066-71issue
3eissn
0308-8146issn
1873-7072pii
S0308-8146(13)00708-5journal_volume
141pub_type
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