Abstract:
:This study investigated a method for the validation and determination of measurement uncertainty for the simultaneous determination of synthetic phenolic antioxidants (SPAs) such as propyl gallate (PG), octyl gallate (OG), dodecyl gallate (DG), 2,4,5-trihydroxy butyrophenone (THBP), tert-butylhydroquinone (TBHQ), butylated hydroxyanisole (BHA), and butylated hydroxytoluene (BHT) in edible oils commonly consumed in Korea. The validated method was able to extract SPA residues under the optimized HPLC-UV and LC-MS/MS conditions. Furthermore, the measurement of uncertainty was evaluated based on the precision study. For HPLC-UV analysis, the recoveries of SPAs ranged from 91.4% to 115.9% with relative standard deviations between 0.3% and 11.4%. In addition, the expanded uncertainties of the SPAs ranged from 0.15 to 5.91. These results indicate that the validated method is appropriate for the extraction and determination of SPAs and can be used to verify the safety of edible oil products containing SPAs residues.
journal_name
Food Chemjournal_title
Food chemistryauthors
Kim JM,Choi SH,Shin GH,Lee JH,Kang SR,Lee KY,Lim HS,Kang TS,Lee OHdoi
10.1016/j.foodchem.2016.06.053subject
Has Abstractpub_date
2016-12-15 00:00:00pages
19-25eissn
0308-8146issn
1873-7072pii
S0308-8146(16)30946-3journal_volume
213pub_type
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