Abstract:
:A method for the synthesis and purification of 6beta-iodomethyl-19-norcholest-5(10)-ene-3beta-ol-131I of greater than 98 mole% chemical purity and greater than 99% radiochemical purity is presented. Carbon-13 and proton NMR were used to establish the identity and purity. Discrepancies in the characterization of this compound, previously published by two other research groups, are discussed.
journal_name
Steroidsjournal_title
Steroidsauthors
Scott KN,Couch MW,Mareci TH,Williams CMdoi
10.1016/0039-128x(76)90117-3subject
Has Abstractpub_date
1976-08-01 00:00:00pages
295-303issue
2eissn
0039-128Xissn
1878-5867pii
0039-128X(76)90117-3journal_volume
28pub_type
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