Abstract:
:A highly selective approach to produce levulinic acid from cellulose was developed via microwave-assisted synthesis in SO3H-functionalized ionic liquids (SFILs). The effects of reaction conditions and ionic liquid structures on the yield of levulinic acid have been investigated, where the highest yield of 55.0% was obtained. The catalytic activities of SFILs depend on the anions and decrease in the order: HSO4->CH3SO3->H2PO4-, which is in good agreement with their acidity order. The SFILs are efficient catalysts for cellulose conversion into levulinic acid and the subsequent esterification, which facilitates the separation of product and reuse of ionic liquids.
journal_name
Bioresour Technoljournal_title
Bioresource technologyauthors
Ren H,Zhou Y,Liu Ldoi
10.1016/j.biortech.2012.12.132subject
Has Abstractpub_date
2013-02-01 00:00:00pages
616-9eissn
0960-8524issn
1873-2976pii
S0960-8524(12)01990-6journal_volume
129pub_type
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