Influence of Conditioning Time of Universal Adhesives on Adhesive Properties and Enamel-Etching Pattern.

Abstract:

OBJECTIVES:To evaluate the effect of application protocol in resin-enamel microshear bond strength (μSBS), in situ degree of conversion, and etching pattern of three universal adhesive systems. METHODS AND MATERIALS:Sixty-three extracted third molars were sectioned in four parts (buccal, lingual, and proximals) and divided into nine groups, according to the combination of the main factors-Adhesive (Clearfil Universal, Kuraray Noritake Dental Inc, Tokyo, Japan; Futurabond U, VOCO, Cuxhaven, Germany; and Scotchbond Universal Adhesive, 3M ESPE, St Paul, MN, USA)-and enamel treatment/application time (etch-and-rinse mode [ER], self-etch [SE] application for 20 seconds [SE20], and SE application for 40 seconds [SE40]). Specimens were stored in water (37°C/24 h) and tested at 1.0 mm/min (μSBS). The degree of conversion of the adhesives at the resin-enamel interfaces was evaluated using micro-Raman spectroscopy. The enamel-etching pattern was evaluated under a scanning electron microscope. Data were analyzed with two-way analysis of variance and Tukey test (α=0.05). RESULTS:In general, the application of the universal adhesives in the SE40 produced μSBS and degree of conversion that were higher than in the SE20 (p<0.01) and similar to the ER mode. The deepest enamel-etching pattern was obtained in the ER mode, followed by the SE40. CONCLUSIONS:The active and prolonged application of universal adhesives in the SE mode may be a viable alternative to increase the degree of conversion, etching pattern, and resin-enamel bond strength.

journal_name

Oper Dent

journal_title

Operative dentistry

authors

Cardenas AM,Siqueira F,Rocha J,Szesz AL,Anwar M,El-Askary F,Reis A,Loguercio A

doi

10.2341/15-213-L

subject

Has Abstract

pub_date

2016-09-01 00:00:00

pages

481-490

issue

5

eissn

0361-7734

issn

1559-2863

journal_volume

41

pub_type

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