Abstract:
:We wish to describe further developments to a method previously reported on the detection of 2-phenoxyethanol in ink. The solid-phase microextraction (SPME) sampling technique, together with gas chromatography-mass spectrometry (GC-MS), has been used to quantify solvents in writing ink. In conventional approaches, the analysis of ink on documents requires some degree of destructive sampling. The methods commonly used remove ink samples from paper using a scalpel or a paper punch. To avoid document destruction, a sampling cell was constructed that allows solvents to be adsorbed directly onto the SPME fiber from the headspace above the document surface. Analytes (ink volatiles) are then desorbed from the SPME fiber on a gas chromatograph equipped with a mass selective detector (GC-MSD). With this method, it was possible to detect the presence of ink solvents on documents for a period lasting up to c. 2 years.
journal_name
J Forensic Scijournal_title
Journal of forensic sciencesauthors
Brazeau L,Gaudreau Mdoi
10.1111/j.1556-4029.2006.00299.xsubject
Has Abstractpub_date
2007-01-01 00:00:00pages
209-15issue
1eissn
0022-1198issn
1556-4029pii
JFO299journal_volume
52pub_type
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