Abstract：
:Anticoagulant rodenticides are widely used for rodent control around the world. A rapid and sensitive method was developed and validated for the simultaneous determination of 13 anticoagulant rodenticides (coumafuryl, pindone, valone, warfarin, coumatetralyl, coumachlor, diphacinone, dicumarol, chlorophacinone, bromadiolone, difenacoum, flocoumafen, and brodifacoum) in human blood by liquid chromatography-tandem mass spectrometry. After liquid-liquid extraction, the anticoagulant rodenticides were separated on an Eclipse Plus C18 column. Linearities were observed for each analyte in blood ranging from 0.5 to 50 ng/mL, with correlation coefficients over 0.99. The limits of detection ranged from 0.01 to 0.2 ng/mL, and the limits of quantification were 0.5 ng/mL for all analytes. The intraday and interday precisions were <15%, and accuracies ranged from 80.3% to 111.0%. This validated method with high sensitivity has been applied in three anticoagulant rodenticide poisoning cases and has been used successfully in monitoring blood concentrations for months.
journal_name
J Forensic Scijournal_title
Journal of forensic sciencesauthors
Qiao Z,Xiang P,Shen B,Shen M,Yan Hdoi
10.1111/1556-4029.13613subject
Has Abstractpub_date
2018-05-01 00:00:00pages
784-792issue
3eissn
0022-1198issn
1556-4029journal_volume
63pub_type
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journal_title：Journal of forensic sciences
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doi：10.1111/1556-4029.13826
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journal_title：Journal of forensic sciences
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doi：10.1111/j.1556-4029.2011.01702.x
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journal_title：Journal of forensic sciences
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更新日期：1987-09-01 00:00:00
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journal_title：Journal of forensic sciences
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更新日期：1997-03-01 00:00:00
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journal_title：Journal of forensic sciences
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更新日期：2003-07-01 00:00:00
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journal_title：Journal of forensic sciences
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doi：
更新日期：1979-01-01 00:00:00
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journal_title：Journal of forensic sciences
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doi：
更新日期：1983-10-01 00:00:00
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journal_title：Journal of forensic sciences
pub_type： 杂志文章
doi：
更新日期：1986-07-01 00:00:00
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journal_title：Journal of forensic sciences
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更新日期：1978-07-01 00:00:00
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journal_title：Journal of forensic sciences
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journal_title：Journal of forensic sciences
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更新日期：1999-05-01 00:00:00
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journal_title：Journal of forensic sciences
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journal_title：Journal of forensic sciences
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journal_title：Journal of forensic sciences
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journal_title：Journal of forensic sciences
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journal_title：Journal of forensic sciences
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更新日期：2002-01-01 00:00:00
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journal_title：Journal of forensic sciences
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journal_title：Journal of forensic sciences
pub_type： 杂志文章
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journal_title：Journal of forensic sciences
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更新日期：2000-05-01 00:00:00
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journal_title：Journal of forensic sciences
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