Abstract：
:A forensic procedure for the quantitative confirmation of lysergic acid diethylamide (LSD) and the qualitative confirmation of its metabolite, N-demethyl-LSD, in blood, serum, plasma, and urine samples is presented. The Zymark RapidTrace was used to perform fully automated solid-phase extractions of all specimen types. After extract evaporation, confirmations were performed using liquid chromatography (LC) followed by positive electrospray ionization (ESI+) mass spectrometry/mass spectrometry (MS/MS) without derivatization. Quantitation of LSD was accomplished using LSD-d3 as an internal standard. The limit of quantitation (LOQ) for LSD was 0.05 ng/mL. The limit of detection (LOD) for both LSD and N-demethyl-LSD was 0.025 ng/mL. The recovery of LSD was greater than 95% at levels of 0.1 ng/mL and 2.0 ng/mL. For LSD at 1.0 ng/mL, the within-run and between-run (different day) relative standard deviation (RSD) was 2.2% and 4.4%, respectively.
journal_name
J Forensic Scijournal_title
Journal of forensic sciencesauthors
de Kanel J,Vickery WE,Waldner B,Monahan RM,Diamond FXsubject
Has Abstractpub_date
1998-05-01 00:00:00pages
622-5issue
3eissn
0022-1198issn
1556-4029journal_volume
43pub_type
杂志文章abstract：:The combination of photographs taken at two or three wavelengths at and bracketing an absorbance peak indicative of a particular compound can lead to an image with enhanced visualization of the compound. This procedure works best for compounds with absorbance bands that are narrow compared with "average" chromophores....
journal_title：Journal of forensic sciences
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abstract：:A blind quality control (QC) program was successfully developed and implemented in the Toxicology, Seized Drugs, Firearms, Latent Prints (Processing and Comparison), Forensic Biology, and Multimedia (Digital and Audio/Video) sections at the Houston Forensic Science Center (HFSC). The program was put into practice base...
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journal_title：Journal of forensic sciences
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journal_title：Journal of forensic sciences
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journal_title：Journal of forensic sciences
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journal_title：Journal of forensic sciences
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更新日期：2001-11-01 00:00:00
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journal_title：Journal of forensic sciences
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更新日期：1997-09-01 00:00:00
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journal_title：Journal of forensic sciences
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更新日期：1976-04-01 00:00:00
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journal_title：Journal of forensic sciences
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journal_title：Journal of forensic sciences
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journal_title：Journal of forensic sciences
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doi：
更新日期：1992-09-01 00:00:00
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journal_title：Journal of forensic sciences
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更新日期：1997-07-01 00:00:00
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更新日期：1997-09-01 00:00:00
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journal_title：Journal of forensic sciences
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更新日期：1997-07-01 00:00:00
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journal_title：Journal of forensic sciences
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journal_title：Journal of forensic sciences
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journal_title：Journal of forensic sciences
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更新日期：2003-11-01 00:00:00
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journal_title：Journal of forensic sciences
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更新日期：1994-11-01 00:00:00
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journal_title：Journal of forensic sciences
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更新日期：2001-09-01 00:00:00
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journal_title：Journal of forensic sciences
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更新日期：1978-04-01 00:00:00
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journal_title：Journal of forensic sciences
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更新日期：2000-11-01 00:00:00
abstract：:A new set of multiplexed PCR primers has been applied to the analysis of human skeletal remains to determine their efficacy in analyzing degraded DNA. These primer sets, known as Miniplexes, produce shorter amplicons (50-280 base pairs (bp)) than standard short tandem repeat (STR) kits, but still utilize the 13 CODIS ...
journal_title：Journal of forensic sciences
pub_type： 杂志文章
doi：10.1111/j.1556-4029.2006.00077.x
更新日期：2006-03-01 00:00:00
