Graphite furnace atomic absorption elemental analysis of ecstasy tablets.

Abstract:

:Six metals (copper, magnesium, barium, nickel, chromium and lead) were determined in two separate batches of seized ecstasy tablets by graphite furnace atomic absorption spectroscopy (GFAAS) following digestion with nitric acid and hydrogen peroxide. Large intra-batch variations were found as expected for tablets produced in clandestine laboratories. For example, nickel in batch 1 was present in the range 0.47-13.1 parts per million (ppm) and in batch 2 in the range 0.35-9.06 ppm. Although batch 1 had significantly higher 3,4-methylenedioxy-N-methamphetamine (MDMA) content than batch 2, barium was the only element which discriminated between the two ecstasy seizures (batch 1: 0.19-0.66 ppm, batch 2: 3.77-5.47 ppm).

journal_name

Forensic Sci Int

authors

French HE,Went MJ,Gibson SJ

doi

10.1016/j.forsciint.2013.04.021

subject

Has Abstract

pub_date

2013-09-10 00:00:00

pages

88-91

issue

1-3

eissn

0379-0738

issn

1872-6283

pii

S0379-0738(13)00244-2

journal_volume

231

pub_type

杂志文章
  • Unexpected natural death secondary to intra-abdominal bleeding: report of one idiopathic spontaneous intraperitoneal hemorrhage case.

    abstract::A 39-year-old woman was found dead at home. She was single, foreign national, chronic alcoholic, and had given shelter to a compatriot for three days. This man found the deceased in her bed, after a night of heavy drinking. The emergency medical team observed numerous recent blue ecchymoses of the upper limbs. Because...

    journal_title:Forensic science international

    pub_type: 杂志文章

    doi:10.1016/j.forsciint.2011.08.004

    authors: Dedouit F,Piercecchi-Marti MD,Leonetti G,Rougé D,Telmon N

    更新日期:2012-01-10 00:00:00

  • Studies on the use of isoelectric focusing as a method of phenotyping erythrocyte acid phosphatase.

    abstract::The technique of isoelectric focusing (IEF) in ultra-thin polyacrylamide gels as a method of phenotyping erythrocyte acid phosphatase (EAP) has been applied to a large number of red cell lysate and dried bloodstains. This paper presents the results of this study and discusses some features of the IEF patterns and prob...

    journal_title:Forensic science international

    pub_type: 杂志文章

    doi:10.1016/0379-0738(81)90141-9

    authors: Divall GB

    更新日期:1981-07-01 00:00:00

  • Genetic profile of the Açores Archipelago population using the new PowerPlex 16 system kit.

    abstract::Allele and haplotype frequencies of 16 chromosome STR loci, 15 of them included in the Kit PowerPlex16 System from Promega were determined in a sample of unrelated males from the Açores Archipelago. All subjects were subjected to an interview in order to make sure that their ancestors belonged to the same island at le...

    journal_title:Forensic science international

    pub_type: 杂志文章

    doi:10.1016/s0379-0738(02)00203-7

    authors: Velosa RG,Fernandes AT,Brehm A

    更新日期:2002-09-10 00:00:00

  • GPR and ERT detection and characterization of a mass burial, Spanish Civil War, Northern Spain.

    abstract::Around 27,000 people were killed in the province of Asturias during the Spanish Civil War, with several thousands killed after the war ended. There are currently over 2,000 known mass burial locations throughout Spain, but many more are unknown. Geophysics is a useful tool employed to help in the active attempts to do...

    journal_title:Forensic science international

    pub_type: 历史文章,杂志文章

    doi:10.1016/j.forsciint.2018.03.034

    authors: Rubio-Melendi D,Gonzalez-Quirós A,Roberts D,García García MDC,Caunedo Domínguez A,Pringle JK,Fernández-Álvarez JP

    更新日期:2018-06-01 00:00:00

  • Sudden death from ruptured septic myocardial infarct in an intravenous drug addict.

    abstract::A case of ruptured septic myocardial infarct with death from cardiac tamponade in an intravenous drug addict with left-sided infective endocarditis and septic coronary artery embolism is described. To the best of our knowledge, there is no previous report of such a case in the literature. Although uncommon, infective ...

    journal_title:Forensic science international

    pub_type: 杂志文章

    doi:10.1016/0379-0738(95)01779-i

    authors: Dickens P,Ho J,Wong KY

    更新日期:1995-08-28 00:00:00

  • Forensic analysis of condom traces: Chemical considerations and review of the literature.

    abstract::The analysis of condom traces has recently been added to the standard forensic examination protocol of sexual assault and rape cases. Several recent studies have thus focussed on the detection of condom components and classification of the chemical profiles using statistics, obtaining very promising results. The purpo...

    journal_title:Forensic science international

    pub_type: 杂志文章,评审

    doi:10.1016/j.forsciint.2020.110255

    authors: Burnier C,Massonnet G

    更新日期:2020-05-01 00:00:00

  • A simple spectrophotometric method for the determination of carboxyhemoglobin in blood.

    abstract::The spectrophotometric method for the determination of carboxyhemoglobin (HbCO) in blood reported by Fretwurst and Meinecke was modified so as to give the same values of percentage HbCO (HbCO%) as those determined by the oxygen electrode method. Values of HbCO% of nine practical samples determined by both the oxygen e...

    journal_title:Forensic science international

    pub_type: 杂志文章

    doi:10.1016/0379-0738(81)90157-2

    authors: Katsumata Y,Aoki M,Sato K,Oya M,Yada S,Suzuki O

    更新日期:1981-09-01 00:00:00

  • Chemical profiling of the street cocktail drug 'nyaope' in South Africa using GC-MS II: Stability studies of the cannabinoid, opiate and antiretroviral components during sample storage.

    abstract::Nyaope is a mixture of low grade heroin, cannabis products, antiretroviral drugs and other materials added as bulking agents. It is a highly physically additive mixture which is smoked by users. As part of the development of a method for the analysis and profiling of nyaope this study evaluates the stability of the ca...

    journal_title:Forensic science international

    pub_type: 杂志文章

    doi:10.1016/j.forsciint.2019.04.040

    authors: Mthembi PM,Mwenesongole EM,Cole MD

    更新日期:2019-07-01 00:00:00

  • On the interpretation of likelihood ratios in forensic science evidence: Presentation formats and the weak evidence effect.

    abstract::Likelihood ratios are increasingly being adopted to convey expert evaluative opinions to courts. In the absence of appropriate databases, many of these likelihood ratios will include verbal rather than numerical estimates of the support offered by the analysis. However evidence suggests that verbal formulations of unc...

    journal_title:Forensic science international

    pub_type: 杂志文章

    doi:10.1016/j.forsciint.2014.04.005

    authors: Martire KA,Kemp RI,Sayle M,Newell BR

    更新日期:2014-07-01 00:00:00

  • A modified method for examining the cardiac conduction system.

    abstract::A revised technique is described in which the sino-atrial node, the atrio-ventricular node and the distal part of the His bundle and the bundle brances of the cardiac conduction system are demonstrated in longitudinal sections through cutting of 4-5 blocks. The longitudinal sectioning allows observation of continuity ...

    journal_title:Forensic science international

    pub_type: 杂志文章

    doi:10.1016/s0379-0738(97)00047-9

    authors: Song Y,Zhu J,Laaksonen H,Saukko P

    更新日期:1997-04-18 00:00:00

  • A rapid and simplified extraction of haloperidol from plasma or serum with bond elut C18 cartridge for analysis by high performance liquid chromatography.

    abstract::This method for the determination of haloperidol (HAL) in plasma is based on high-performance liquid chromatography (HPLC) with a reversed-phase column, ODS-C18. HAL is rapidly extracted from human plasma by using Bond Elut C18 cartridge and its recovery is over 90%. The mobile phase is a mixture of 1% acetate/acetoni...

    journal_title:Forensic science international

    pub_type: 杂志文章

    doi:10.1016/0379-0738(87)90025-9

    authors: Hayakari M,Hashimoto Y,Kita T,Murakami S

    更新日期:1987-09-01 00:00:00

  • Using whole exome sequencing and bioformatics in the molecular autopsy of a sudden unexplained death syndrome (SUDS) case.

    abstract::Whole exome sequencing (WES) and bioinformatics analysis were used to investigate potential disease-causing gene mutations in a sudden unexplained death syndrome (SUDS) case after autopsy and pathology tests failed to suggest an obvious disease mechanism. Following whole exome sequencing, a 3-step bioinformatics filte...

    journal_title:Forensic science international

    pub_type: 杂志文章

    doi:10.1016/j.forsciint.2015.08.022

    authors: Wang C,Duan S,Lv G,Lai X,Chen R,Lin H,Qiu S,Tang J,Kuang W,Xu C

    更新日期:2015-12-01 00:00:00

  • Identification of unknown dead bodies by X-ray image comparison of the skull using the X-ray simulation program FoXSIS.

    abstract::The aim of the study was to improve the objectivity of X-ray image comparison for the identification of unknown dead individuals. CT-data were collected for 30 macerated skulls. An already presented computer program which uses CT data to establish virtual X-ray images was used to obtain X-rays with different beam angu...

    journal_title:Forensic science international

    pub_type: 杂志文章

    doi:10.1016/s0379-0738(00)00452-7

    authors: Riepert T,Ulmcke D,Schweden F,Nafe B

    更新日期:2001-03-01 00:00:00

  • Right heart ischemia in cases of sepsis.

    abstract::Data from the literature suggest that cases of sepsis complicated by right ventricular (RV) dysfunction have poorer prognosis. In these cases progressive hypoperfusion associated to increasing, injury-related, pulmonary vascular resistance account for RV ischemia. In the present analysis, we wanted to evaluate whether...

    journal_title:Forensic science international

    pub_type: 杂志文章

    doi:10.1016/j.forsciint.2015.12.002

    authors: Fracasso T,Jentgens L,Pfeiffer H,Sauerland C,Mangin P,Schmeling A

    更新日期:2016-02-01 00:00:00

  • Analysis of 15 STR loci in Chinese population from Sichuan in West China.

    abstract::Allele frequencies for 15 STR loci found in PowerPlex 16 System kit were determined in a sample of 200 unrelated individuals living in Sichuan area in west China. The values of observed heterozygosity (Ho), power of discrimination (PD), probability of paternity exclusion (PE) and polymorphism information content (PIC)...

    journal_title:Forensic science international

    pub_type: 杂志文章

    doi:10.1016/j.forsciint.2006.05.039

    authors: Zhang H,Li Y,Jiang J,Zhang J,Wu J,Du H,Yan J,Shen Y,Hou Y

    更新日期:2007-09-13 00:00:00

  • Using subsampling to estimate the strength of handwriting evidence via score-based likelihood ratios.

    abstract::The likelihood ratio paradigm has been studied as a means for quantifying the strength of evidence for a variety of forensic evidence types. Although the concept of a likelihood ratio as a comparison of the plausibility of evidence under two propositions (or hypotheses) is straightforward, a number of issues arise whe...

    journal_title:Forensic science international

    pub_type: 杂志文章

    doi:10.1016/j.forsciint.2011.09.013

    authors: Davis LJ,Saunders CP,Hepler A,Buscaglia J

    更新日期:2012-03-10 00:00:00

  • Fatal embolism of the anterior spinal artery after local cervical analgetic infiltration.

    abstract::A 66-year-old man received a local infiltration of cortisone and xylocain in the left paravertebral region between the fifth and sixth cervical vertebrae. Respiratory failure occurred 2.5 h later with subsequent successful resuscitation. During the following 2 months of assisted ventilation up to the patients death, t...

    journal_title:Forensic science international

    pub_type: 杂志文章

    doi:10.1016/j.forsciint.2004.05.018

    authors: Meyer HJ,Monticelli F,Kiesslich J

    更新日期:2005-05-10 00:00:00

  • Testing for ethanol markers in hair: discrepancies after simultaneous quantification of ethyl glucuronide and fatty acid ethyl esters.

    abstract::The hair of 97 cases were analysed for ethyl glucuronide (EtG) and fatty acid ethyl esters (FAEE, including ethyl myristate, ethyl palmitate, ethyl oleate and ethyl stearate) according to the Society of Hair Testing guidelines to examine the role of both tests in documenting chronic excessive alcohol drinking, particu...

    journal_title:Forensic science international

    pub_type: 杂志文章

    doi:10.1016/j.forsciint.2014.03.012

    authors: Kintz P,Nicholson D

    更新日期:2014-10-01 00:00:00

  • Determination of synthesis route of 1-(3,4-methylenedioxyphenyl)-2-propanone (MDP-2-P) based on impurity profiles of MDMA.

    abstract::In our study 1-(3,4-methylenedioxyphenyl)-2-propanone (MDP-2-P or PMK) was prepared by two different routes, i.e. by oxidizing isosafrole in an acid medium and by 1-(3,4-methylenedioxyphenyl)-2-nitropropene reduction. The final product-MDP-2-P was subjected to GC/MS analysis. The intermediates and reaction by-products...

    journal_title:Forensic science international

    pub_type: 杂志文章

    doi:10.1016/j.forsciint.2004.06.016

    authors: Swist M,Wilamowski J,Zuba D,Kochana J,Parczewski A

    更新日期:2005-05-10 00:00:00

  • The use of ventral fusion between sacral elements S1 and S2 as an additional age-at-death indicator in a black South African skeletal sample.

    abstract::Despite indicating numerous demographic features such as sex, stature, and age; the sacrum remains a relatively insufficiently researched skeletal element. A set pattern of ossification and fusion of the sacrum makes it a useful bone for estimating age-at-death in unknown skeletal individuals. The aims of this study, ...

    journal_title:Forensic science international

    pub_type: 杂志文章

    doi:10.1016/j.forsciint.2018.02.011

    authors: Mahon TJ,Friedling LJ,Gordon GM

    更新日期:2018-05-01 00:00:00

  • Traffic injury or attempted infanticide?

    abstract::Two sewing needles were found in a woman's cranial cavity by X-ray examination after she had sustained traffic injury. After investigation and analysis, it has been confirmed that the sewing needles were inserted by others when she was an infant, and not by the traffic injury. ...

    journal_title:Forensic science international

    pub_type: 杂志文章

    doi:10.1016/s0379-0738(01)00470-4

    authors: Meng X

    更新日期:2001-10-15 00:00:00

  • Y chromosomal short tandem repeat (STR) loci in a representative group of males living in South Württemberg: a database for application in forensic medicine.

    abstract::In this study, we resolved the allelic distribution of three Y chromosomal short tandem repeats (STRs), DYS19 (n=218), DYS390 (n=257) and DYS393 (n=215), in a population study of 257 unrelated men living in the area of South Wüerttemberg/Hohenzollern. In DYS19 and in DYS393, five different alleles were discovered, and...

    journal_title:Forensic science international

    pub_type: 杂志文章

    doi:10.1016/s0379-0738(00)00195-x

    authors: Graw M,Seitz T

    更新日期:2000-09-11 00:00:00

  • A new method for detecting diatoms in human organs.

    abstract::A new method for diatom detection is described. It includes an ultrasonic irradiation procedure with the use of a tissue solubilizer. The method is easy to carry out and is less time-consuming than previous techniques. ...

    journal_title:Forensic science international

    pub_type: 杂志文章

    doi:10.1016/0379-0738(80)90181-4

    authors: Fukui Y,Hata M,Takahashi S,Matsubara K

    更新日期:1980-07-01 00:00:00

  • Influence of rain and malathion on the oviposition and development of blowflies (Diptera: Calliphoridae) infesting rabbit carcasses in Kelantan, Malaysia.

    abstract::The influence of rain and malathion on the initial oviposition as well as development of blowfly species infesting rabbit carcasses decomposing in sunlit and shaded habitats were studied over a period of 1 year in Kelantan, Malaysia. Chrysomya megacephala (Fabricius) was the most dominant species that infested the car...

    journal_title:Forensic science international

    pub_type: 杂志文章

    doi:10.1016/j.forsciint.2009.07.008

    authors: Mahat NA,Zafarina Z,Jayaprakash PT

    更新日期:2009-11-20 00:00:00

  • New alleles and mutational events in D12S391 and D8S1132: sequence data from an eastern German population.

    abstract::To investigate the DNA mutation rate and pattern in the hypervariable short tandem repeat (STR) locus D12S391 and in the locus D8S1132, samples from an eastern German population (Dresden area) were analysed. A duplex PCR was applied, using short amplification products for D12S391 (129-177bp) and a modified reverse pri...

    journal_title:Forensic science international

    pub_type: 杂志文章

    doi:10.1016/s0379-0738(01)00596-5

    authors: Hering S,Müller E

    更新日期:2001-12-27 00:00:00

  • Evaluating the evidentiary value of the analysis of skeletal trauma in forensic research: A review of research and practice.

    abstract::Understanding bone trauma characteristics is a fundamental component of forensic investigations that can assist in understanding the nature of blunt trauma related deaths. The variation of each blunt force trauma (BFT) injury is dependent on a magnitude of factors including, age, sex, health, angle of impact, impact m...

    journal_title:Forensic science international

    pub_type: 杂志文章,评审

    doi:10.1016/j.forsciint.2020.110140

    authors: Dempsey N,Blau S

    更新日期:2020-02-01 00:00:00

  • Comparing roadside with subsequent breath alcohol analyses and their relevance to the issue of retrograde extrapolation.

    abstract::Driving while intoxicated (DWI) legislation requires proving the critical breath alcohol concentration (BrAC) at the time of driving. With time delayed analysis, retrograde extrapolation is occasionally employed but has several uncertainties associated with it. The present study attempts to address whether subjects ac...

    journal_title:Forensic science international

    pub_type: 杂志文章

    doi:10.1016/0379-0738(92)90013-m

    authors: Gullberg RG,McElroy AJ

    更新日期:1992-12-01 00:00:00

  • Hair concentrations and self-reported abuse history of 20 amphetamine and ecstasy users.

    abstract::Hair samples of 20 volunteers of the techno-music scene, who more or less regularly consumed ecstasy tablets and speed and anonymously reported their abuse history, were analyzed in one to seven 3 cm segments for amphetamine (A), methamphetamine (MA), methylenedioxyamphetamine (MDA), methylenedioxymethamphetamine (MDM...

    journal_title:Forensic science international

    pub_type: 杂志文章

    doi:10.1016/s0379-0738(97)00123-0

    authors: Rothe M,Pragst F,Spiegel K,Harrach T,Fischer K,Kunkel J

    更新日期:1997-09-19 00:00:00

  • Genetic variation at eight STR loci in the Korean population.

    abstract::The frequency distributions of eight STR loci were surveyed in 510 unrelated individuals from the Korean population ...

    journal_title:Forensic science international

    pub_type: 杂志文章

    doi:10.1016/s0379-0738(00)00334-0

    authors: Han MS,Kang PW,Choi DH,Lee YH,Choi SK,Kim W

    更新日期:2001-02-01 00:00:00

  • Utilizing AFIS searching tools to reduce errors in fingerprint casework.

    abstract::Fifty-six (56) adjudicated, property crime cases involving fingerprint evidence were reviewed using a case-specific AFIS database tool. This tool allowed fingerprint experts to search latent prints in the cases against a database of friction ridge exemplars limited to only the individuals specific to that particular c...

    journal_title:Forensic science international

    pub_type: 杂志文章

    doi:10.1016/j.forsciint.2015.07.054

    authors: Langenburg G,Hall C,Rosemarie Q

    更新日期:2015-12-01 00:00:00