An improvement in sintering property of beta-tricalcium phosphate by addition of calcium pyrophosphate.

Abstract:

:The sintering behavior of calcium pyrophosphate (CPP, Ca2P2O7)-doped beta-tricalcium phosphate [TCP, Ca3(PO4)2], prepared by solid state reaction, was investigated in-situ, using dilatometry. Pure beta-TCP undergoes phase transition to alpha-TCP at about 1200 degrees C; hence pure beta-TCP ceramics should be sintered bclow 1200 degrees C. Pure beta-TCP sintered body can achieve a relative density of only 86% when sintered at 1150 degrees C. However, the addition of CPP in the range of 0.5-3 wt% delays phasc transition of beta-TCP and enables sintering of beta-TCP at 1200 degrees C without a phase transformation to alpha-TCP. Due to this effect of CPP added to TCP, CPP-doped beta-TCP ceramics with relative density over 95% could be obtained when sintered at 1200 degrees C for 2 h.

journal_name

Biomaterials

journal_title

Biomaterials

authors

Ryu HS,Youn HJ,Hong KS,Chang BS,Lee CK,Chung SS

doi

10.1016/s0142-9612(01)00201-0

keywords:

subject

Has Abstract

pub_date

2002-02-01 00:00:00

pages

909-14

issue

3

eissn

0142-9612

issn

1878-5905

pii

S0142-9612(01)00201-0

journal_volume

23

pub_type

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