Abstract:
:A mixture of four tetracyclines; oxytetracycline (OTC), chlortetracycline (CTC), tetracycline (TC), and doxycycline (DC) was applied in fifteen 12000l outdoor microcosms at four treatment levels plus controls each with three replicates (n = 3). The dissipation times of parent compounds were monitored and half-lives (DT50) of 1-4 days, depending on treatment level were recorded. This is in accordance with half-lives from previous findings in bench-top experiments. Parent compound DT50, were determined using HPLC-UV. Furthermore, the samples were analyzed for ten different tetracycline products using LC/MS/MS. Two products were found for chlortetracycline; 4-epi-anh-chlortetracyline and the iso-chlortetracycline. Iso-forms were only found for CTC and only at the highest treatment (300 microg l(-1)). The half-lives, trajectories, and relative amounts of the products were analogous for all four tetracyclines. DT50 for products were less than 1.2 days. Formation of 4-epi-anh-tetracyclines, occurred at neutral to weak alkaline conditions.
journal_name
Chemospherejournal_title
Chemosphereauthors
Sanderson H,Ingerslev F,Brain RA,Halling-Sørensen B,Bestari JK,Wilson CJ,Johnson DJ,Solomon KRdoi
10.1016/j.chemosphere.2005.01.035subject
Has Abstractpub_date
2005-07-01 00:00:00pages
619-29issue
5eissn
0045-6535issn
1879-1298pii
S0045-6535(05)00177-3journal_volume
60pub_type
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