Application of Focused Ultrasound-Assisted Extraction for the Quantification of Persistent Organic Pollutions in Liver Tissue of Giant Toad (Rhinella marina).

Abstract:

:A simple and rapid focused ultrasound extraction method was developed for the determination of Persistent Organic Pollutants (POPs) in liver tissue obtained of giant toad (Rhinella marina) using a gas chromatography coupled to a mass detector with electron impact ionization. The performed method for POPs, was validated in fortified matrix, showing linearity from the LOQ up to 100 ng/mL; LODs and LOQs for each compound were between 1.7 and 4.8 and 3.5-7.5 ng/mL, respectively. Recovery rates were among 79%-116% for POPs determined. Finally, the method was applied in liver samples of giant toads found in a malarial area in Mexico. The sensitivity of the proposed method was good enough to ensure reliable determination of target analytes at concentration levels commonly found in this kind of samples.

authors

Flores-Ramírez R,Espinosa-Reyes G,Cilia-López VG,González-Mille DJ,Rodríguez-Aguilar M,Díaz de León-Martínez L,Díaz-Barriga F

doi

10.1007/s00128-016-2009-y

subject

Has Abstract

pub_date

2017-02-01 00:00:00

pages

204-211

issue

2

eissn

0007-4861

issn

1432-0800

pii

10.1007/s00128-016-2009-y

journal_volume

98

pub_type

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