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Transesterification of edible, non-edible and used cooking oils for biodiesel production using calcined layered double hydroxides as reusable base catalysts.

Abstract：

:Fatty acid methyl esters (FAME) were produced from edible, non-edible and used cooking oils with different fatty acid contents by transesterification with methanol using calcined layered double hydroxides (LDHs) as solid base catalysts. Among the catalysts, calcined CaAl2-LDH (hydrocalumite) showed the highest activity with >90% yield of FAME using low methanol:oil molar ratio (<6:1) at 65 °C in 5 h. The activity of the catalyst was attributed to its high basicity as supported by Hammett studies and CO(2)-TPD measurements. The catalyst was successfully reused in up to four cycles. Some of the properties such as density, viscosity, neutralization number and glycerol content of the obtained biodiesel matched well with the standard DIN values. It is concluded that a scalable heterogeneously catalyzed process for production of biodiesel in high yields from a wide variety of triglyceride oils including used oils is possible using optimized conditions.

journal_name

Bioresour Technol

journal_title

Bioresource technology

authors

Sankaranarayanan S,Antonyraj CA,Kannan S

doi

10.1016/j.biortech.2012.01.022

subject

Has Abstract

pub_date

2012-04-01 00:00:00

pages

57-62

eissn

0960-8524

issn

1873-2976

pii

S0960-8524(12)00028-4

journal_volume

109

pub_type

杂志文章

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