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Optimization of furfural and 5-hydroxymethylfurfural production from wheat straw by a microwave-assisted process.

Abstract：

:Optimization of acid-catalyzed conversion conditions of wheat straw into furfural, 5-hydroxymethylfurfural (HMF), glucose, and xylose was studied by response surface methodology (RSM). A central composite design (CCD) was used to determine the effects of independent variables, including reaction temperature (140-200 °C), residence time (1-41 min), pH (0.1-2.1), and liquid:solid ratio (15-195 mL/g) on furan and sugar production. The surface response analysis revealed that temperature, time and pH had a strong influence on the furfural, HMF, xylose and glucose yield, whereas liquid to solid ratio was found not to be significant. The initial pH of solution was the most important variable in acid-catalyzed conversion of wheat straw to furans. The maximum predicted furfural, HMF, xylose and glucose yields were 66%, 3.4%, 100%, and 65%, respectively. This study demonstrated that the microwave-assisted process was a very effective method for the xylose production from wheat straw by diluted acid catalysis.

journal_name

Bioresour Technol

journal_title

Bioresource technology

authors

Yemiş O,Mazza G

doi

10.1016/j.biortech.2012.01.031

subject

Has Abstract

pub_date

2012-04-01 00:00:00

pages

215-23

eissn

0960-8524

issn

1873-2976

pii

S0960-8524(12)00037-5

journal_volume

109

pub_type

杂志文章

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