Magnetic solid-phase extraction based on graphene oxide for the determination of lignans in sesame oil.

Abstract:

:Graphene oxide was fabricated by a simple method and applied to magnetic solid-phase extraction. In a pretreatment procedure before the sesamol, sesamin and sesamolin in sesame oil were detected by high performance liquid chromatography. Several parameters affecting the extraction efficiency were investigated, including the type and volume of desorption solvent, desorption time and the amount of sorbent. Under the optimized conditions, the detection limits of sesamol, sesamin, and sesamolin were 0.05μg/g, 0.02μg/g, and 0.02μg/g, respectively. The limits of quantification were all 0.2μg/g. The average recoveries of sesamol, sesamin, and sesamolin were 84.55%, 85.47%, 86.83%, respectively and their relative standard deviations were 1.23%, 1.33%, and 0.84%, respectively.

journal_name

Food Chem

journal_title

Food chemistry

authors

Wu L,Yu L,Ding X,Li P,Dai X,Chen X,Zhou H,Bai Y,Ding J

doi

10.1016/j.foodchem.2016.08.109

subject

Has Abstract

pub_date

2017-02-15 00:00:00

pages

320-325

eissn

0308-8146

issn

1873-7072

pii

S0308-8146(16)31349-8

journal_volume

217

pub_type

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