Microwave plasma atomic emission spectrometric determination of Ca, K and Mg in various cheese varieties.

Abstract:

:Microwave plasma-atomic emission spectrometry (MP-AES) was used to determine calcium, magnesium and potassium in various Turkish cheese samples. Cheese samples were dried at 100 °C for 2 days and then digested in a mixture of nitric acid/hydrogen peroxide (3:1). Good linearities (R(2) > 0.999) were obtained up to 10 μg mL(-1) of Ca, Mg and K at 445.478 nm, 285.213 nm and 766.491 nm, respectively. The analytes in a certified reference milk powder sample were determined within the uncertainty limits. Moreover, the analytes added to the cheese samples were recovered quantitatively (>90%). All determinations were performed using aqueous standards for calibration. The LOD values for Ca, Mg and K were 0.036 μg mL(-1), 0.012 μg mL(-1) and 0.190 μg mL(-1), respectively. Concentrations of Ca, K and Mg in various types of cheese samples produced in different regions of Turkey were found between 1.03-3.70, 0.242-0.784 and 0.081-0.303 g kg(-1), respectively.

journal_name

Food Chem

journal_title

Food chemistry

authors

Ozbek N,Akman S

doi

10.1016/j.foodchem.2015.07.011

subject

Has Abstract

pub_date

2016-02-01 00:00:00

pages

295-8

eissn

0308-8146

issn

1873-7072

pii

S0308-8146(15)01016-X

journal_volume

192

pub_type

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