Abstract:
:In this work, we show how the water flip-back approach that is widely employed in solution-state NMR can be adapted to proton-detected MAS solid-state NMR of highly deuterated proteins. The scheme allows to enhance the sensitivity of the experiment by decreasing the recovery time of the proton longitudinal magnetization. The method relies on polarization transfer from non-saturated water to the protein during the inter-scan delay.
journal_name
J Biomol NMRjournal_title
Journal of biomolecular NMRauthors
Chevelkov V,Xiang S,Giller K,Becker S,Lange A,Reif Bdoi
10.1007/s10858-015-9902-2subject
Has Abstractpub_date
2015-02-01 00:00:00pages
151-60issue
2eissn
0925-2738issn
1573-5001journal_volume
61pub_type
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