Abstract:
:A continuous-flow integration process was developed for biodiesel production using rapeseed oil as feedstock, based on the countercurrent contact reaction between gas and liquid, separation of glycerol on-line and cyclic utilization of methanol. Orthogonal experimental design and response surface methodology were adopted to optimize technological parameters. A second-order polynomial model for the biodiesel yield was established and validated experimentally. The high determination coefficient (R(2)=98.98%) and the low probability value (Pr<0.0001) proved that the model matched the experimental data, and had a high predictive ability. The optimal technological parameters were: 81.5°C reaction temperature, 51.7cm fill height of catalyst KF/CaO and 105.98kPa system pressure. Under these conditions, the average yield of triplicate experiments was 93.7%, indicating the continuous-flow process has good potential in the manufacture of biodiesel.
journal_name
Bioresour Technoljournal_title
Bioresource technologyauthors
Hu S,Wen L,Wang Y,Zheng X,Han Hdoi
10.1016/j.biortech.2012.05.143subject
Has Abstractpub_date
2012-11-01 00:00:00pages
413-8eissn
0960-8524issn
1873-2976pii
S0960-8524(12)01036-Xjournal_volume
123pub_type
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