Chemiluminescence determination of terbutaline sulfate in bovine urine and pharmaceutical preparations based on enhancement of the 2-phenyl-4, 5-di (2-furyl) imidazole-potassium ferricyanide system.

Abstract:

:In this paper, a novel chemiluminescence (CL) system, 2-phenyl-4, 5-di (2-furyl) imidazole (PDFI)-potassium ferricyanide, for the determination of terbutaline sulfate was described. The method was based on enhancement of CL emission of PDFI-potassium ferricyanide system in the presence of terbutaline sulfate. Under the optimum conditions, the enhanced chemiluminescence intensity is linearly related to the concentration of terbutaline sulfate. The proposed method has been successfully applied to the determination of terbutaline sulfate in bovine urine and pharmaceutical preparations with satisfactory results. Furthermore, the possible mechanism of chemiluminescence reaction was also discussed briefly.

journal_name

J Pharm Biomed Anal

authors

Han L,Zhang Y,Kang J,Tang J,Zhang Y

doi

10.1016/j.jpba.2011.09.011

subject

Has Abstract

pub_date

2012-01-25 00:00:00

pages

141-5

eissn

0731-7085

issn

1873-264X

pii

S0731-7085(11)00529-2

journal_volume

58

pub_type

杂志文章
  • Quantitation of tenofovir and emtricitabine in dried blood spots (DBS) with LC-MS/MS.

    abstract::A reversed-phase high performance liquid chromatographic (LC), tandem mass spectrometry (MS/MS) assay for the determination of tenofovir (TFV) and emtricitabine (FTC) in dried blood spots (DBS) from human whole blood was developed and validated. Whole blood samples were spotted, dried, and a 3mm punch was extracted wi...

    journal_title:Journal of pharmaceutical and biomedical analysis

    pub_type: 杂志文章

    doi:10.1016/j.jpba.2013.08.033

    authors: Zheng JH,Guida LA,Rower C,Castillo-Mancilla J,Meditz A,Klein B,Kerr BJ,Langness J,Bushman L,Kiser J,Anderson PL

    更新日期:2014-01-01 00:00:00

  • Pharmacokinetic and pharmacodynamic study of imidaprilat, an active metabolite of imidapril, a new angiotensin-converting enzyme inhibitor, in spontaneously hypertensive rats.

    abstract::The pharmacokinetics and pharmacodynamics (PK/PD) of imidaprilat, an active metabolite of imidapril, a new angiotensin-converting enzyme (ACE) inhibitor, were investigated. Imidapril was infused subcutaneously for 4 weeks via an osmotic pump implanted under the skin in the back of male spontaneously hypertensive rats ...

    journal_title:Journal of pharmaceutical and biomedical analysis

    pub_type: 杂志文章

    doi:10.1016/s0731-7085(96)02015-8

    authors: Yamanaka K,Takehara N,Murata K,Banno K,Sato T

    更新日期:1997-08-01 00:00:00

  • Preparation and the kinetic stability of hyaluronan radiolabeled with 111In, 125I and 14C.

    abstract::Three different procedures for the labeling of hyaluronan (HA) with (111)In, (125)I and (14)C radionuclides were compared, and the kinetic stability of radiolabeled HA under different conditions (saline, artificial gastric juice and plasma) was established. Modification of HA structure with bifunctional chelating agen...

    journal_title:Journal of pharmaceutical and biomedical analysis

    pub_type: 杂志文章

    doi:10.1016/j.jpba.2010.02.005

    authors: Cozikova D,Laznickova A,Hermannova M,Svanovsky E,Palek L,Buffa R,Sedova P,Koppova R,Petrik M,Smejkalova D,Laznicek M,Velebny V

    更新日期:2010-08-01 00:00:00

  • Serum metabolomics reveals the mechanistic role of functional foods and exercise for obesity management in rats.

    abstract::Obesity is one of the independent risk factors for several health problems, leading to metabolic perturbations and for which analytical approaches i.e., "metabolomics" is needed to monitor the underlying metabolic changes. In this study, obesity associated changes were assessed via serum metabolites analysis of obese ...

    journal_title:Journal of pharmaceutical and biomedical analysis

    pub_type: 杂志文章

    doi:10.1016/j.jpba.2017.05.001

    authors: Ammar NM,Farag MA,Kholeif TE,Metwally NS,El-Sheikh NM,El Gendy AN,Abdel-Hamid AZ

    更新日期:2017-08-05 00:00:00

  • Portable near-infrared instruments: Application for quality control of polymorphs in pharmaceutical raw materials and calibration transfer.

    abstract::This work presents an evaluation of the analytical performance of three different portable near-infrared (NIR) instruments (denominated Port.1, Port.2 and Port.3) for quantifying mebendazole polymorphs (A, B and C) in pharmaceutical raw materials using multivariate calibration models. The performance of the portable i...

    journal_title:Journal of pharmaceutical and biomedical analysis

    pub_type: 杂志文章

    doi:10.1016/j.jpba.2016.11.036

    authors: da Silva VH,da Silva JJ,Pereira CF

    更新日期:2017-02-05 00:00:00

  • Stability of ricobendazole in aqueous solutions.

    abstract::The chemical stability of ricobendazole (RBZ) was investigated using a stability-indicating high performance liquid chromatographic (HPLC) assay with ultraviolet detection. The degradation kinetics of RBZ in aqueous solution was evaluated as a function of pH, buffer strength and temperature. The oxidation reaction in ...

    journal_title:Journal of pharmaceutical and biomedical analysis

    pub_type: 杂志文章

    doi:10.1016/j.jpba.2009.02.032

    authors: Wu Z,Tucker IG,Razzak M,Medlicott NJ

    更新日期:2009-07-12 00:00:00

  • Difference spectrophotometric assay of 5-hydroxymethylfurfuraldehyde in hydrolysed pharmaceutical syrups-II. Isoniazid reagent.

    abstract::A rapid difference spectrophotometric assay of 5-hydroxymethylfurfuraldehyde (5-HMF) in certain degraded syrups is described. The method involves the measurement of the difference absorbance at 340 nm of the isonicotinoyl hydrazone of 5-HMF, formed at room temperature in an acidic solution of isoniazid, relative to an...

    journal_title:Journal of pharmaceutical and biomedical analysis

    pub_type: 杂志文章

    doi:10.1016/0731-7085(88)80030-x

    authors: Davidson AG,Dawodu TO

    更新日期:1988-01-01 00:00:00

  • Metabolites identification of berberine in rats using ultra-high performance liquid chromatography/quadrupole time-of-flight mass spectrometry.

    abstract::Berberine (BBR), the principle component for many medicinal plants such as Coptis chinensis Franch., Phellodendron chinense Schneid., and Mahonia bealei (Fort.) Carr., possesses diverse pharmacological activities, including anti-bacterial, anti-inflammatory, antitumor, hypolipidemic and antidiabetic activities. In thi...

    journal_title:Journal of pharmaceutical and biomedical analysis

    pub_type: 杂志文章

    doi:10.1016/j.jpba.2017.02.038

    authors: Wang K,Chai L,Feng X,Liu Z,Liu H,Ding L,Qiu F

    更新日期:2017-05-30 00:00:00

  • Release of proteolytic activity following reduction in therapeutic human serum albumin containing products: detection with a new neoepitope endopeptidase immunoassay.

    abstract::Botulinum type A toxin (BoNT/A) is defined by its specific endopeptidase cleavage of SNAP25 between Gln(197) and Arg(198) under reducing conditions. The neurotoxin is widely used for therapeutic or cosmetic purposes, but should not contain other toxin serotypes or unwanted protease activities. Using a neoepitope endop...

    journal_title:Journal of pharmaceutical and biomedical analysis

    pub_type: 杂志文章

    doi:10.1016/j.jpba.2010.08.013

    authors: Jones RG,Liu Y,Halls C,Thorpe SJ,Longstaff C,Matejtschuk P,Sesardic D

    更新日期:2011-01-05 00:00:00

  • Inhibitory assay for degradation of collagen IV by cathepsin B with a surface plasmon resonance sensor.

    abstract::We describe a simple method for evaluating the inhibition of collagen IV degradation by cathepsin B with a surface plasmon resonance (SPR) biosensor. The change in the SPR signal decreased with an increase in the concentration of cathepsin B inhibitors. The order of the inhibitory constant (Ki) obtained by the SPR met...

    journal_title:Journal of pharmaceutical and biomedical analysis

    pub_type: 杂志文章

    doi:10.1016/j.jpba.2017.06.026

    authors: Shoji A,Suenaga Y,Hosaka A,Ishida Y,Yanagida A,Sugawara M

    更新日期:2017-10-25 00:00:00

  • Electrochemical DNA nano-biosensor for the study of spermidine-DNA interaction.

    abstract::An electrochemical DNA nano-biosensor is prepared by immobilization of double stranded DNA (dsDNA) onto a mixed self-assembled monolayer (SAM) composed of azide- and hydroxyl-terminated thiols. The SAMs- and dsDNA-modified gold electrodes were characterized by cyclic voltammetry (CV) and electrochemical impedance spec...

    journal_title:Journal of pharmaceutical and biomedical analysis

    pub_type: 杂志文章

    doi:10.1016/j.jpba.2008.12.035

    authors: Mehdinia A,Kazemi SH,Bathaie SZ,Alizadeh A,Shamsipur M,Mousavi MF

    更新日期:2009-04-05 00:00:00

  • Development and validation of a high-performance liquid chromatographic stability-indicating method for the analysis of Synercid in quality control, stability and compatibility studies.

    abstract::A gradient high-performance liquid chromatographic (HPLC) method was developed for the analysis of Synercid freeze-dried powder in routine quality control, stability and compatibility studies. This method is suited for a simultaneous assay of drug substances and impurities. The method was validated for precision, repr...

    journal_title:Journal of pharmaceutical and biomedical analysis

    pub_type: 杂志文章

    doi:10.1016/s0731-7085(98)00242-8

    authors: Vasselle B,Gousset G,Bounine JP

    更新日期:1999-04-01 00:00:00

  • HPLC method for the determination and pharmacokinetic studies on puerarin in cerebral ischemia reperfusion rat plasma after intravenous administration of puerariae radix isoflavone.

    abstract::A new HPLC method for the determination of puerarin in cerebral ischemia reperfusion rat plasma is introduced. Puerarin, the principal bioactive component of puerariae radix isoflavone, was extracted from plasma by methanol. The HPLC separation was then performed on a reversed-phase C18 column using water-acetonitrile...

    journal_title:Journal of pharmaceutical and biomedical analysis

    pub_type: 杂志文章

    doi:10.1016/j.jpba.2004.10.046

    authors: Yan B,Xing D,Ding Y,Tao J,Du LJ

    更新日期:2005-02-23 00:00:00

  • Identification of a new tadalafil analogue in an adulterated dietary supplement: trans-Bisprehomotadalafil.

    abstract::A new tadalafil analogue was identified along with homotadalafil during routine screening of an adulterated dietary supplement using HPLC-DAD. The UV spectrum of this analogue was almost identical with that of tadalafil. This compound was isolated from the supplement by using semi-preparative HPLC and its structure wa...

    journal_title:Journal of pharmaceutical and biomedical analysis

    pub_type: 杂志文章

    doi:10.1016/j.jpba.2015.07.023

    authors: Lee JH,Kim HJ,Mandava S,Hwang J,Park HJ,Cho S,Baek SY,Lee J

    更新日期:2015-11-10 00:00:00

  • Analysis of cationic liposomes by reversed-phase HPLC with evaporative light-scattering detection.

    abstract::Cationic lipid-mediated drug delivery of small pharmaceutical molecules and biological molecules, such as proteins and DNA, has gained increasing popularity for many in vitro and in vivo applications. For this purpose, 1,2-dioleoyl-3-trimethylammonium propane (DOTAP) is one of the most widely used and efficient cation...

    journal_title:Journal of pharmaceutical and biomedical analysis

    pub_type: 杂志文章

    doi:10.1016/j.jpba.2009.10.001

    authors: Zhong Z,Ji Q,Zhang JA

    更新日期:2010-03-11 00:00:00

  • Pharmacokinetic and tissue distribution studies of 1,9-pyrazoloanthrone, a c-Jun-N-terminal kinase inhibitor in Wistar rats by a simple and sensitive HPLC method.

    abstract::JNK pathway activates c-Jun(s) which are responsible for cell apoptosis; as a result, inhibitors of JNK pathway have the potential to prevent dopaminergic neurons from death and decrease the loss of dopamine in substantia nigra pars compacta (SNpc). Recent in-vitro studies show that 1,9-pyrazoloanthrone (1,9-P) a pote...

    journal_title:Journal of pharmaceutical and biomedical analysis

    pub_type: 杂志文章

    doi:10.1016/j.jpba.2015.12.004

    authors: Ambhore NS,Yamjala K,Mohire S,Raju KR,Mulukutla S,Murthy V,Tondhawada M,Elango K

    更新日期:2016-02-20 00:00:00

  • Estimation of impurity profiles of drugs and related materials. Part 14: the role of HPLC/diode-array UV spectroscopy in the identification of minor components (impurities, degradation products, metabolites) in various matrices.

    abstract::The possibility of the rapid identification of drug related minor components by HPLC/diode-array UV spectroscopy is demonstrated by three examples. Hydroxylated impurities (degradation products) of norgestrel (6 alpha and beta, 10 beta-hydroxy derivatives) were identified on the basis of their UV spectra and retention...

    journal_title:Journal of pharmaceutical and biomedical analysis

    pub_type: 杂志文章

    doi:10.1016/0731-7085(95)01579-5

    authors: Görög S,Bihari M,Csizér E,Dravetz F,Gazdag M,Herényi B

    更新日期:1995-12-01 00:00:00

  • A preliminary study of beta-cyclodextrin/metoprolol tartrate inclusion complex for potential enantiomeric separation.

    abstract::The inclusion complex formation between Metoprolol tartarata (MeT) and beta-cyclodextrin (beta-CD) has been investigated using hyperchromic shift at lambda(max) 274.4 nm of MeT. Different parameters such as stirring time, solvent composition (aqueous and aqueous/methanol solutions with methanol content up to 50%), pH ...

    journal_title:Journal of pharmaceutical and biomedical analysis

    pub_type: 杂志文章

    doi:10.1016/s0731-7085(00)00555-0

    authors: Radulovic DM,Karljikovic-Rajic KD,Lucic BM,Vujic ZB

    更新日期:2001-03-01 00:00:00

  • Capillary electrophoresis for caffeine and pyroglutamate determination in coffees study of the in vivo effect on learning and locomotor activity in mice.

    abstract::In a preliminary study pyroglutamate showed to be over 10 times increased in some lyophilised coffees with respect to brewed or filtered coffees, and probably that increase is related to some stage of the industrial process. Pyroglutamate is known to have a number of remarkable cognitive enhancing effects, which could...

    journal_title:Journal of pharmaceutical and biomedical analysis

    pub_type: 杂志文章

    doi:10.1016/j.jpba.2006.01.062

    authors: Maeso N,del Castillo C,Cornejo L,García-Acicollar M,Alguacil LF,Barbas C

    更新日期:2006-06-16 00:00:00

  • Multicomponent spectrophotometric assay of riboflavine and photoproducts.

    abstract::A multicomponent spectrophotometric method has been developed for the simultaneous determination of riboflavine, formylmethylflavine and degradation products in photolysed solutions. It is based on partial separation of the photoproducts by chloroform extraction at pH 2.0 in a potassium chloride-hydrochloric acid solu...

    journal_title:Journal of pharmaceutical and biomedical analysis

    pub_type: 杂志文章

    doi:10.1016/0731-7085(90)80029-o

    authors: Ahmad I,Rapson HD

    更新日期:1990-01-01 00:00:00

  • Assessment of antipyrine kinetics from saliva or plasma: influence of age.

    abstract::The purpose of this study was to investigate whether antipyrine estimation in saliva provides valid information on plasma antipyrine clearance (APCl) and can be useful as an index of changes in drug metabolism with age. Antipyrine kinetics was studied in 93 elderly (mean age 82 years) and 23 young (mean age 29 years) ...

    journal_title:Journal of pharmaceutical and biomedical analysis

    pub_type: 临床试验,杂志文章

    doi:10.1016/0731-7085(95)01531-o

    authors: Jorquera F,Almar MM,Jimeno A,González-Sastre M,González-Gallego J

    更新日期:1995-08-01 00:00:00

  • Determination of 2-hydroxyphenylacetic acid (2HPAA) in urine after oral and parenteral administration of coumarin by gas-liquid chromatography with flame-ionization detection.

    abstract::The urinary excretion of 2-hydroxyphenylacetic acid (2HPAA) was studied in human volunteers after oral and parenteral doses of coumarin. The presence of 2HPAA in the urine was confirmed by gas chromatography mass spectroscopy (GC MS). Mass spectra of reference material and samples are presented. The determination of 2...

    journal_title:Journal of pharmaceutical and biomedical analysis

    pub_type: 杂志文章

    doi:10.1016/s0731-7085(97)00224-0

    authors: Meineke I,Desel H,Kahl R,Kahl GF,Gundert-Remy U

    更新日期:1998-07-01 00:00:00

  • Determination of the ionization constants of 4-iodo-2,6-dimethylphenylcarbamoylmethyl iminodiacetic acid.

    abstract::In order to develop a radiopharmaceutical for hepatobiliary scintigraphy with better hepatobiliary properties new ligand for complexation of 99mTc, 4-iodo-2,6-dimethylphenylcarbamoylmethyl iminodiacetic acid (METHYLIODIDA), was synthesized. Acid-base equilibria of METHYLIODIDA were studied potentiometrically, because ...

    journal_title:Journal of pharmaceutical and biomedical analysis

    pub_type: 杂志文章

    doi:10.1016/j.jpba.2004.03.009

    authors: Jovanović MS,Popović G,Kapetanović V,Orlić M,Vladimirov S

    更新日期:2004-09-03 00:00:00

  • In vivo and in vitro metabolism of the designer anabolic steroid furazadrol in thoroughbred racehorses.

    abstract::Furazadrol ([1',2']isoxazolo[4',5':2,3]-5α-androstan-17β-ol) is a designer anabolic androgenic steroid that is readily available via the internet. It contains an isoxazole fused to the steroid A-ring which offers metabolic stability and noteworthy anabolic activity raising concerns over the potential for abuse of this...

    journal_title:Journal of pharmaceutical and biomedical analysis

    pub_type: 杂志文章

    doi:10.1016/j.jpba.2016.02.031

    authors: Waller CC,Cawley AT,Suann CJ,Ma P,McLeod MD

    更新日期:2016-05-30 00:00:00

  • Analytical techniques for characterization of cyclodextrin complexes in the solid state: A review.

    abstract::Cyclodextrins are cyclic oligosaccharides able to form inclusion complexes with a variety of hydrophobic guest molecules, positively modifying their physicochemical properties. A thorough analytical characterization of cyclodextrin complexes is of fundamental importance to provide an adequate support in selection of t...

    journal_title:Journal of pharmaceutical and biomedical analysis

    pub_type: 杂志文章,评审

    doi:10.1016/j.jpba.2015.01.058

    authors: Mura P

    更新日期:2015-09-10 00:00:00

  • Evaluation of sample work-up methods and internal standards for the determination of 5-hydroxytryptamine and 5-hydroxyindoleacetic acid in brain by HPLC with electrochemical detection.

    abstract::A high-performance liquid chromatographic method with electrochemical detection is described for the determination of 5-hydroxytryptamine (5-HT) and 5-hydroxyindoleacetic acid (5-HIAA) in brain. Results of studies on sample work-up methods and on the use of various internal standards are reported. The reproducibility ...

    journal_title:Journal of pharmaceutical and biomedical analysis

    pub_type: 杂志文章

    doi:10.1016/0731-7085(88)80108-0

    authors: Duchateau A,Martens H,Teuchy H,Schoups A,Claeys M

    更新日期:1988-01-01 00:00:00

  • Stability-indicating UPLC method for determination of Valsartan and their degradation products in active pharmaceutical ingredient and pharmaceutical dosage forms.

    abstract::A simple, precise, accurate stability-indicating gradient reverse phase ultra-performance liquid chromatographic (RP-UPLC) method was developed for the quantitative determination of purity of Valsartan drug substance and drug products in bulk samples and pharmaceutical dosage forms in the presence of its impurities an...

    journal_title:Journal of pharmaceutical and biomedical analysis

    pub_type: 杂志文章

    doi:10.1016/j.jpba.2010.05.022

    authors: Krishnaiah Ch,Reddy AR,Kumar R,Mukkanti K

    更新日期:2010-11-02 00:00:00

  • Determination of cocaine and benzoylecgonine by direct injection of human urine into a column-switching liquid chromatography system with diode-array detection.

    abstract::A method for the determination of cocaine (COC) and benzoylecgonine (BZE) in human urine using a column-switching liquid chromatography system is reported. A homemade precolumn (20 mm x 4.6 mm i.d.) dry-packed with Alltech ODS-C18 (35-750 microm) was employed as an extraction precolumn in order to extract and concentr...

    journal_title:Journal of pharmaceutical and biomedical analysis

    pub_type: 杂志文章

    doi:10.1016/j.jpba.2004.09.048

    authors: Brunetto MR,Delgado Cayama Y,Gutiérrez García L,Gallignani M,Obando MA

    更新日期:2005-02-07 00:00:00

  • A spectroscopic investigation of DuP 747 polymorphs.

    abstract::DuP 747, a selective kappa agonist analgesic, was found to have at least two polymorphic forms, and this was confirmed by X-ray powder diffraction. DSC and thermomicroscopic studies indicated the polymorphic pair to be monotropic. Solubility studies suggested the relative stability of the two forms to be similar. The ...

    journal_title:Journal of pharmaceutical and biomedical analysis

    pub_type: 杂志文章

    doi:10.1016/0731-7085(94)e0002-i

    authors: Raghavan K,Dwivedi A,Campbell GC Jr,Nemeth G,Hussain MA

    更新日期:1994-06-01 00:00:00

  • Myoglobin microplate assay to evaluate prevention of protein peroxidation.

    abstract::The current therapeutic strategies are based on the design of multifunctional drug candidates able to interact with various disease related targets. Drugs that have the ability to scavenge reactive oxygen species (ROS), beyond their main therapeutic action, may prevent the oxidative damage of biomolecules. Therefore, ...

    journal_title:Journal of pharmaceutical and biomedical analysis

    pub_type: 杂志文章

    doi:10.1016/j.jpba.2015.06.006

    authors: Marques SS,Magalhães LM,Mota AI,Soares TR,Korsak B,Reis S,Segundo MA

    更新日期:2015-10-10 00:00:00