Abstract:
:In this study, sulphated zirconia was directly synthesised and compared to the conventional wet method of preparation. The surface areas and pore sizes were 169 m(2)/g, 0.61 μm (directly synthesized) and 65 m(2)/g, 0.24 μm (conventional method), respectively. Directly synthesized sulphated zirconia was amorphous, whereas conventionally prepared sulphated zirconia is polycrystalline. Their IR spectra were broadly similar, although the area of the 1250 to 950 cm(-1) band was larger for directly synthesised sulphated zirconia. Not only were conversions greater for directly synthesised sulphated zirconia (63% vs. 42% after 4h), but it exhibited significantly greater yield for fatty acid methyl esters. The percentage yield (after 1h) of methyl esters was 43% for the directly synthesised catalyst and 15% for the conventionally synthesised.
journal_name
Bioresour Technoljournal_title
Bioresource technologyauthors
Eterigho EJ,Lee JG,Harvey APdoi
10.1016/j.biortech.2011.02.040subject
Has Abstractpub_date
2011-05-01 00:00:00pages
6313-6issue
10eissn
0960-8524issn
1873-2976pii
S0960-8524(11)00225-2journal_volume
102pub_type
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