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River bottom sediment from the Vistula as matrix of candidate for a new reference material.

Abstract：

:Bottom sediments are very important in aquatic ecosystems. The sediments accumulate heavy metals and compounds belonging to the group of persistent organic pollutants. The accelerated solvent extraction (ASE) was used for extraction of 16 compounds from PAH group from bottom sediment of Vistula. For the matrix of candidate of a new reference material, moisture content, particle size, loss on ignition, pH, and total organic carbon were determined. A gas chromatograph with a selective mass detector (GC/MS) was used for the final analysis. The obtained recoveries were from 86% (SD=6.9) for anthracene to 119% (SD=5.4) for dibenzo(ah)anthracene. For the candidate for a new reference material, homogeneity and analytes content were determined using a validated method. The results are a very important part of the development and certification of a new reference materials.

journal_name

Ecotoxicol Environ Saf

journal_title

Ecotoxicology and environmental safety

authors

Kiełbasa A,Buszewski B

doi

10.1016/j.ecoenv.2017.03.007

subject

Has Abstract

pub_date

2017-08-01 00:00:00

pages

237-242

eissn

0147-6513

issn

1090-2414

pii

S0147-6513(17)30141-0

journal_volume

142

pub_type

杂志文章

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