Abstract:
:QuEChERS and solid phase extraction (SPE) methods were optimized and applied for the extraction of triazines in fruit and vegetables. These extraction methods are easy, effective, rugged and safe. Also, they have the ability to purify the extracts which leads to lower detection limits and higher recoveries of the analytes. The analysis were conducted using liquid chromatography coupled to photodiode array detector. The limits of detection and quantification ranged from 0.4 -1.4 µg/kg and 1.5 - 4.5 µg/kg, respectively, for QuEChERS and 0.3 - 1.8 µg/kg and 1.4 - 4.9 µg/kg respectively, for SPE. The recoveries ranged from 84 to 102% for QuEChERS and 76-119% for SPE, with relative standard deviation less than 20% for both methods. The fruits and vegetables analysed were apples, pears, carrots, potatoes, tomatoes, avocado, cucumber, spinach, bananas, and oranges. The concentrations detected ranged between 6 and 46 µg/kg in fruits and 4 - 84 µg/kg in vegetables. Simazine was detected in all fruits and vegetable samples except in pear, while terbutylazine was not detected in all samples analysed. Propazine and ametryn were only found in carrot while pear sample only had atrazine. The proposed methods proved to be sensitive and accurate indicating their applicability for detection and monitoring of the selected triazines in fruits and vegetables. However, QuEChERS can be recommended for routine analysis of these triazines due to its fewer extraction steps compared to SPE which is important for turn-around time.
journal_name
Food Chemjournal_title
Food chemistryauthors
Mnyandu HM,Mahlambi PNdoi
10.1016/j.foodchem.2021.129818keywords:
["Fruit and vegetables","Liquid chromatography","Photodiode array","QuEChERS","Solid phase extraction","Triazine herbicides"]subject
Has Abstractpub_date
2021-10-30 00:00:00pages
129818eissn
0308-8146issn
1873-7072pii
S0308-8146(21)00824-4journal_volume
360pub_type
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