Abstract:
:The characterization of inorganic elements in the produced water (PW) samples is a difficult task because of the complexity of the matrix. This work deals with a study of a methodology for dissolved Fe quantification in PW from oil industry by flame atomic absorption spectrometry (FAAS) after cloud point extraction (CPE). The procedure is based on the CPE using PAN as complexing agent and Triton X-114 as surfactant. The best conditions for Fe extraction parameters were studied using a Box-Behnken design. The proposed method presented a LOQ of 0.010μgmL-1 and LOD of 0.003μgmL-1. The precision of the method was evaluated in terms of repeatability, obtaining a coefficient of variation of 2.54%. The accuracy of the method was assessed by recovery experiments of Fe spiked that presented recovery of 103.28%. The method was applied with satisfactory performance to determine Fe by FAAS in PW samples.
journal_name
Mar Pollut Bulljournal_title
Marine pollution bulletinauthors
Gondim TA,Guedes JA,Ribeiro LP,Lopes GS,Matos WOdoi
10.1016/j.marpolbul.2016.10.068subject
Has Abstractpub_date
2017-01-30 00:00:00pages
786-791issue
2eissn
0025-326Xissn
1879-3363pii
S0025-326X(16)30890-6journal_volume
114pub_type
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