Comparison of supercritical fluid extraction and solvent extraction of twenty-two organochlorine pesticides from eggs.

Abstract:

:The recoveries of twenty-two organochlorine pesticides spiked in egg samples were extracted by supercritical fluid extraction (SFE) using carbon dioxide and solvent extraction using acetonitrile were compared. The extracts were cleaned up with C18 and Florisil SPE columns. At 0.1 ppm spike level, the recoveries were 52 - 100% by SFE and 53 - 93% by solvent extraction. The limits of detection calculated at 0.01 ppm spike level were 0.072 - 0.006 ppm for SFE and 0.06 - 0.006 ppm for solvent extraction. Both methods show improvement in sample preparation time and solvent consumption from the existing Soxhlet extraction method.

journal_name

Chemosphere

journal_title

Chemosphere

authors

Wigfield YY,Selwyn J,Khan S,McDowell R

doi

10.1016/0045-6535(96)00021-5

subject

Has Abstract

pub_date

1996-03-01 00:00:00

pages

841-7

issue

5

eissn

0045-6535

issn

1879-1298

pii

0045653596000215

journal_volume

32

pub_type

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