Multiresidue determination of organophorous pesticides in camellia oil by matrix solid-phase dispersion followed by GC-FPD.

Abstract:

:A novel analytical approach has been developed and evaluated for the quantitative analysis of 15 organophorous pesticides residues in camellia oils. The proposed methodology is based on acetonitrile/water (3:1, V/V) extraction, followed by matrix solid-phase dispersion, using aminopropyl as dispersant material. Then gas chromatography-flame photometric detection was applied for the pesticide residue analysis. The optimal sorbent quantity was studied. The results demonstrated that the method achieved acceptable quantitative recoveries of 71.5%-104.2% with relative standard deviations <19%, and the method limit of detection at or below the regulatory maximum residue limits for the pesticides were achieved.

authors

Liu Y,Shen D,Tang F

doi

10.1007/s00128-012-0818-1

subject

Has Abstract

pub_date

2012-11-01 00:00:00

pages

1057-61

issue

5

eissn

0007-4861

issn

1432-0800

journal_volume

89

pub_type

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