Preconcentration technique for the determination of trace elements in natural water samples by ICP-AES.

Abstract:

:A procedure was developed for the determination of Cd, Cu, Zn, Co, Ni, Mn, Pb and Mo in water samples by inductively coupled plasma atomic emission spectrometry (ICP-AES) after preconcentration on a morpholine dithiocarbamate (mor-DTC) supported by bagasse (Saccharam aphisinaram). The sorbed elements were subsequently eluted with 4,M HNO3 and the acid eluates were analysed by ICP-AES. The influence of various parameters such as pH, flow rate of sample, eluent concentration, volume of the sample and volume of eluent were investigated to enhance the sensitivity of the present method. A 20,mL disposable syringe served as preconcentration column. Under the optimal conditions Cd, Cu, Zn, Co, Ni, Mn, Pb and Mo in aqueous sample was concentrated about 100-fold. The sorption recoveries of elements were higher than 99.6%. The method is also applied for the analysis of natural and spiked water samples.

journal_name

Environ Monit Assess

authors

Babu SH,Kumar KS,Suvardhan K,Kiran K,Rekha D,Krishnaiah L,Janardhanam K,Chiranjeevi P

doi

10.1007/s10661-006-9309-3

subject

Has Abstract

pub_date

2007-05-01 00:00:00

pages

241-9

issue

1-3

eissn

0167-6369

issn

1573-2959

journal_volume

128

pub_type

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