Abstract:
:A procedure was developed for the determination of Cd, Cu, Zn, Co, Ni, Mn, Pb and Mo in water samples by inductively coupled plasma atomic emission spectrometry (ICP-AES) after preconcentration on a morpholine dithiocarbamate (mor-DTC) supported by bagasse (Saccharam aphisinaram). The sorbed elements were subsequently eluted with 4,M HNO3 and the acid eluates were analysed by ICP-AES. The influence of various parameters such as pH, flow rate of sample, eluent concentration, volume of the sample and volume of eluent were investigated to enhance the sensitivity of the present method. A 20,mL disposable syringe served as preconcentration column. Under the optimal conditions Cd, Cu, Zn, Co, Ni, Mn, Pb and Mo in aqueous sample was concentrated about 100-fold. The sorption recoveries of elements were higher than 99.6%. The method is also applied for the analysis of natural and spiked water samples.
journal_name
Environ Monit Assessjournal_title
Environmental monitoring and assessmentauthors
Babu SH,Kumar KS,Suvardhan K,Kiran K,Rekha D,Krishnaiah L,Janardhanam K,Chiranjeevi Pdoi
10.1007/s10661-006-9309-3subject
Has Abstractpub_date
2007-05-01 00:00:00pages
241-9issue
1-3eissn
0167-6369issn
1573-2959journal_volume
128pub_type
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