Abstract:
:Glass-ceramic powders with the oxide batch formulation 50wt%SiO2, 20wt%P2O5 and 30wt%CaO were prepared by the sol-gel process using tetraethoxysilane, calcium nitrate and phosphoric acid as raw materials. The obtained gels and powders were characterized by TG-DTA thermal analysis, FTIR analyses and XRD measurements. The results indicated that (1) heating to more than 600 degrees C brought about elimination of -OC2H5 side chains from gels, and formation of a SiO2-based glass network, (2) crystallization such as Ca3(PO4)2 notably occurred in the SiO2-based glass matrix when heated to more than 900 degrees C, (3) -OH groups existed on SiO2-based glass-ceramic surfaces in the temperature region less than 900 degrees C, and (4) the melting point of this composition was more than 1400 degrees C. This study suggests that sol-gel-derived SiO2-based glass-ceramic powder containing P and Ca might be useful as bioactive implant materials.
journal_name
Dent Mater Jjournal_title
Dental materials journalauthors
Taira M,Okazaki M,Takahashi Jdoi
10.4012/dmj.16.117subject
Has Abstractpub_date
1997-12-01 00:00:00pages
117-26issue
2eissn
0287-4547issn
1881-1361journal_volume
16pub_type
杂志文章abstract::This in vitro study aimed to investigate the effects of glass-ionomer and flowable composite liners on the fracture resistance of Class II amalgam and composite restorations. Group 1 cavities were restored with amalgam and Group 4 cavities with nanofill composite after the application of a dentin-bonding agent. For th...
journal_title:Dental materials journal
pub_type: 杂志文章
doi:10.4012/dmj.2013-053
更新日期:2013-01-01 00:00:00
abstract::The behavior of microencapsulated polymerization initiators in dental adhesives is unknown. This study investigated the effects of new microencapsulated initiators in novel, multi-purpose, PMMA-type adhesive resin on the bonding performance and polymerization reactivity. Microencapsulated BPO and 1,3,5-trimethylbarbit...
journal_title:Dental materials journal
pub_type: 杂志文章
doi:10.4012/dmj.27.35
更新日期:2008-01-01 00:00:00
abstract::The aim of this study was to evaluate the trial Teaching Robot for the development of a contact-type measuring apparatus for using directly in the oral cavity. A standard model was used to mimic the dentition by placing an arrangement of three bearing balls. The diameters of the balls were measured. A practical dentit...
journal_title:Dental materials journal
pub_type: 杂志文章
doi:10.4012/dmj.22.168
更新日期:2003-06-01 00:00:00
abstract::We examined the mold filling capacity and microhardness of two industrial 1% Fe titanium alloys: Super-TIX800 (Nippon Steel Corp.) (Fe: 0.910%, O: 0.370%, N: 0.005%) and Super-TIX800N (Nippon Steel Corp.) (Fe: 0.960%, O: 0.300%, N: 0.041%). Two wedge-shaped acrylic patterns (with 30 degrees or 15 degrees angles) were ...
journal_title:Dental materials journal
pub_type: 杂志文章
doi:10.4012/dmj.23.211
更新日期:2004-06-01 00:00:00
abstract::High-power light-curing units have emerged that reduce the time of procedures in dental clinical work. However, patients sometimes complain of pain during the polymerization of composite resin. In this experiment, we investigated how differences in light-curing mode affect the temperature rise during composite resin p...
journal_title:Dental materials journal
pub_type: 杂志文章
doi:10.4012/dmj.2018-158
更新日期:2019-07-31 00:00:00
abstract::This study evaluated the biomineralization and dentinal tubules occlusion abilities of the carboxyl-terminated polyamidoamine dendrimer (PAMAM-COOH) on human demineralized dentin in vivo at different time points. Demineralization dentin model with and without treated with PAMAM-COOH were sutured to the interior side o...
journal_title:Dental materials journal
pub_type: 杂志文章
doi:10.4012/dmj.2015-209
更新日期:2016-01-01 00:00:00
abstract::This study aimed to investigate the in vitro biological response of human dental pulp cells to glass ionomer cement (GIC, Fuji IX GP(®)) containing 2.5% magnesium carbonate apatite (MgCO(3)Ap). MgCO(3)Ap was synthesized by wet method and characterized using FT-IR, XPS, and SEM. Fuji IX GP(®) served as a control. Test ...
journal_title:Dental materials journal
pub_type: 杂志文章
doi:10.4012/dmj.2012-096
更新日期:2012-01-01 00:00:00
abstract::Multi-purpose bonding performance of three kinds of newly synthesized phosphonic acid monomers was investigated. Methacryloxyalkyl or acryloxyalkyl phosphonoacetates of 6-MHPA, 6-AHPA, 10-MDPA were synthesized in 42.8-51.9% yields with a light yellow viscous liquid, and identified as new compounds by 1H NMR, IR, and e...
journal_title:Dental materials journal
pub_type: 杂志文章
doi:10.4012/dmj.26.105
更新日期:2007-01-01 00:00:00
abstract::Finite element analysis was performed to evaluate stress distribution in maxillary central incisors treated endodontically and restored with a post and an all-ceramic crown. Tensile stress at tooth root was analyzed using two-dimensional finite element models with different post diameters and lengths. One post length ...
journal_title:Dental materials journal
pub_type: 杂志文章
doi:10.4012/dmj.25.145
更新日期:2006-03-01 00:00:00
abstract::The biaxial flexural strength and cyclic fatigue biaxial flexural strength of CAD/CAM ceramics polished with #220, 400, 600 and 1000 diamond pads were measured in an effort to determine the effect of surface roughness on fatigue behavior of dental ceramics. The surface roughness was improved after polishing with a sma...
journal_title:Dental materials journal
pub_type: 杂志文章
doi:10.4012/dmj.18.395
更新日期:1999-12-01 00:00:00
abstract::The aim of this study was to evaluate the cytotoxicity of contemporary flowable and paste-like bulk-fill dental composites by using a real-time cell analysis. In the present paper, cytotoxicity levels of five flowable, five paste-like bulk-fill composite materials and one conventional flowable, one conventional paste-...
journal_title:Dental materials journal
pub_type: 杂志文章
doi:10.4012/dmj.2018-336
更新日期:2020-01-31 00:00:00
abstract::This study was evaluating how three desensitizing toothpastes used at home influence the effect associated with desensitizing agents after application in the clinic. Fifty dentine disks measure it permeability and 32 dentine disks with similar permeability levels were selected. Following Dental desensitizer treatment,...
journal_title:Dental materials journal
pub_type: 杂志文章
doi:10.4012/dmj.2019-164
更新日期:2020-09-29 00:00:00
abstract::This study assessed the impact of surface treatments and repair resin reinforcement with zirconium oxide nano-particles (nano-ZrO2) on flexural strength (FS) of repaired denture base. A total of 320 heat-polymerized acrylic resin specimens were prepared and sectioned creating 2-mm gap. According to repair surface trea...
journal_title:Dental materials journal
pub_type: 杂志文章
doi:10.4012/dmj.2018-436
更新日期:2020-06-05 00:00:00
abstract::The kinetic polymerization behavior of 2,2,2-trifluoroethyl methacrylate (TFEMA), 1,1,1,3,3,3-hexafluoroisopropyl methacrylate (HFIPMA), 2,2,2-trifluoroethyl acrylate (TFEA) and 1,1,1,3,3,3-hexafluoroisopropyl acrylate (HFIPA) was determined by isothermal differential scanning calorimetry (DSC) and high-performance li...
journal_title:Dental materials journal
pub_type: 杂志文章
doi:10.4012/dmj.2010-054
更新日期:2010-10-01 00:00:00
abstract::Removable partial dentures (RPDs) with resin-clasp retentive parts, which are known as non-metal-clasp dentures (NMCDs), have been used as alternatives for conventional RPDs with metal clasp, in case of aesthetic prosthodontic treatments. In this study, a profilometer and dynamic micro-indentation tests were used to i...
journal_title:Dental materials journal
pub_type: 杂志文章
doi:10.4012/dmj.2018-012
更新日期:2018-11-30 00:00:00
abstract::To determine the effect of titanium (Ti) surface modification by ultraviolet irradiation (UVI) on the bond strength between Ti and porcelain. Grade 2 Ti plates were allotted to five groups: sandblasted (SA), 15 min UVI (UV), SA+5 min UVI (SA+UV5), SA+10 min UVI (SA+UV10), and SA+15 min UVI (SA+UV15). After surface tre...
journal_title:Dental materials journal
pub_type: 杂志文章
doi:10.4012/dmj.2016-417
更新日期:2018-06-08 00:00:00
abstract::The aim of this investigation was to compare the cleaning and shaping efficiency of Self-adjusting file and Protaper, and to assess the correlation between root canal curvature and working time in mandibular molars using micro-computed tomography. Twenty extracted mandibular molars instrumented with Protaper and Self-...
journal_title:Dental materials journal
pub_type: 杂志文章
doi:10.4012/dmj.2016-255
更新日期:2017-09-26 00:00:00
abstract::The purpose of this study was to evaluate the effect of different polymerization cycles on the flexural strengths and microhardness of two denture base materials (Meliodent and Paladent). Heat-polymerized acrylic resin specimens (65.0 mm long×10.0 mm wide×2.5 mm in height) were prepared using different short and long ...
journal_title:Dental materials journal
pub_type: 杂志文章
doi:10.4012/dmj.2016-023
更新日期:2017-03-31 00:00:00
abstract::Adhesion promoting monomers for dental metals, 5-(4-vinylbenzyl)-2-thiobarbituric acid (5VS), 6- (4-vinylbenzyl-n-propyl) amino-1,3,5-triazine-2,4-dithione (VBATDT) and 9,10-epithiodecyl methacrylate (EP8MA), were synthesized and surface treatment agents were prepared by dissolving each monomer in ethanol or acetone. ...
journal_title:Dental materials journal
pub_type: 杂志文章
doi:10.4012/dmj.22.343
更新日期:2003-09-01 00:00:00
abstract::The secretion of collagen by osteoblasts was observed by scanning electron microscopy (SEM). Osteoblast-like cells were cultured on a CO3apatite-collagen sponge reinforced with a porous HAp frame. After three days' incubation, a number of newly created matrix fibrils, forming a network structure, were observed at the ...
journal_title:Dental materials journal
pub_type: 杂志文章
doi:10.4012/dmj.24.460
更新日期:2005-09-01 00:00:00
abstract::The aim of this study was to investigate and compare the radio-opacity of core materials for all-ceramic restorations, such as zirconia (NANOZR and Y-TZP) and alumina, against commercially pure titanium (cpTi) and aluminum. X-ray images were taken under general settings using an X-ray film. The X-ray film images were ...
journal_title:Dental materials journal
pub_type: 杂志文章
doi:10.4012/dmj.2009-54
更新日期:2010-01-01 00:00:00
abstract::The aim of this study was to develop and evaluate an automatic pH-cycling system, which was intended for performing time-lapse analyses of dental caries. Two single-section specimens prepared from each of the five extracted human incisors were studied under a condition of 3- or 9-cycles/day for seven weeks. Increase o...
journal_title:Dental materials journal
pub_type: 杂志文章
doi:10.4012/dmj.25.280
更新日期:2006-06-01 00:00:00
abstract::The aim of this study was to clarify the effect of heating rate on the development of both transient and residual stresses in investment molds. Solid, cylindrical, gypsum-based molds were modeled and theoretical calculations made of temperature distributions with a constant heating rate. These calculations used experi...
journal_title:Dental materials journal
pub_type: 杂志文章
doi:10.4012/dmj.15.121
更新日期:1996-12-01 00:00:00
abstract::The aim of this study was to evaluate the pH at the surface of active or arrested carious dentin using a micro pH sensor, and to compare the relationship between different pH measurement techniques. Twenty extracted carious teeth were divided into two groups, active or arrested caries, according to predefined clinical...
journal_title:Dental materials journal
pub_type: 杂志文章
doi:10.4012/dmj.25.423
更新日期:2006-09-01 00:00:00
abstract::The study evaluated changes in total enzymatic activity and degradation of demineralized dentin following the application of universal or self-etch adhesives. The universal adhesives -Scotchbond Universal (SU) and All-Bond Universal (ABU) and self-etch adhesives -Adper Easy Bond (EB) and G-aenial Bond (GB) were used f...
journal_title:Dental materials journal
pub_type: 杂志文章
doi:10.4012/dmj.2019-304
更新日期:2020-12-03 00:00:00
abstract::Quaternary ammonium compounds (QACs) have been used widely in medicine, owing to their antimicrobial properties. They also have strong permeability, stable performance, low skin irritation, low toxicity, low corrosion, lasting biological effects and so on, comparing with other antimicrobial agents. At the end of last ...
journal_title:Dental materials journal
pub_type: 杂志文章,评审
doi:10.4012/dmj.2017-096
更新日期:2018-03-30 00:00:00
abstract::Thermal misfit is deemed as one reason for the chipping of veneered zirconia restorations. Aim of the present study was to assess the effect of thermal misfit on the fracture load of veneered zirconia frameworks and to evaluate the applicability of a universal veneering ceramic for both zirconia and titanium framework...
journal_title:Dental materials journal
pub_type: 杂志文章
doi:10.4012/dmj.26.766
更新日期:2007-11-01 00:00:00
abstract::We aimed to establish an experimental animal model to evaluate materials for endodontic therapy. We focused on the biocompatibility of new paste-type zinc oxide-eugenol (ZOE) sealer. The results of this sealer were compared with those of conventional powder/liquid ZOE and eugenol-free sealers. The molars of Wistar rat...
journal_title:Dental materials journal
pub_type: 杂志文章
doi:10.4012/dmj.2010-095
更新日期:2011-01-01 00:00:00
abstract::Resin coating materials have been used for composite resin or provisional restoration in order to prevent plaque accumulation on their surfaces. However, it is not clear whether the coating materials influence attachment of periodontal bacteria. Therefore, we investigated the effect of resin coating materials on the a...
journal_title:Dental materials journal
pub_type: 杂志文章,随机对照试验
doi:10.4012/dmj.2011-164
更新日期:2012-02-03 00:00:00
abstract::The possibility of the segregation under solidification process using a centrifugal casting machine was investigated using an electron probe microanalyzer with elemental distribution map, line analysis and quantitative analysis. When a very small quantity of platinum was added to local molten titanium during the casti...
journal_title:Dental materials journal
pub_type: 杂志文章
doi:10.4012/dmj.15.212
更新日期:1996-12-01 00:00:00