Development of pure certified reference material of stevioside.

Abstract:

:Pure stevioside was extracted from leaves of Stevia rebaudiana (Bertoni) to be used as a reference material in the instrument calibration or method validation process. The mass fraction was determined by comparison between the mass balance method and quantitative nuclear magnetic resonance (qNMR) spectroscopy. The impurities in the sample were analyzed by Karl Fischer titration for moisture content and thermogravimetric analysis for inorganic residue. Homogeneity, together with short term and long term stability, were also studied and the uncertainty was reported. The certified value of this mass fraction is 0.986 ± 0.0019 (k = 2) with 1 year stability.

journal_name

Food Chem

journal_title

Food chemistry

authors

Tangpaisarnkul N,Tuchinda P,Wilairat P,Siripinyanond A,Shiowattana J,Nobsathian S

doi

10.1016/j.foodchem.2018.02.029

subject

Has Abstract

pub_date

2018-07-30 00:00:00

pages

75-80

eissn

0308-8146

issn

1873-7072

pii

S0308-8146(18)30256-5

journal_volume

255

pub_type

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