Abstract:
:Pure stevioside was extracted from leaves of Stevia rebaudiana (Bertoni) to be used as a reference material in the instrument calibration or method validation process. The mass fraction was determined by comparison between the mass balance method and quantitative nuclear magnetic resonance (qNMR) spectroscopy. The impurities in the sample were analyzed by Karl Fischer titration for moisture content and thermogravimetric analysis for inorganic residue. Homogeneity, together with short term and long term stability, were also studied and the uncertainty was reported. The certified value of this mass fraction is 0.986 ± 0.0019 (k = 2) with 1 year stability.
journal_name
Food Chemjournal_title
Food chemistryauthors
Tangpaisarnkul N,Tuchinda P,Wilairat P,Siripinyanond A,Shiowattana J,Nobsathian Sdoi
10.1016/j.foodchem.2018.02.029subject
Has Abstractpub_date
2018-07-30 00:00:00pages
75-80eissn
0308-8146issn
1873-7072pii
S0308-8146(18)30256-5journal_volume
255pub_type
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