Abstract:
:Most commercially available plant celluloses, such as kraft pulps and cotton celluloses, have so-called leveling-off degrees of polymerization (LODPs) when subjected to dilute acid hydrolysis. The formation of LODPs is hypothesized to be caused by disordered regions that are present periodically along each cellulose microfibril in plant celluloses. Here, we prepared never-dried wood cellulose, and wood celluloses at different drying stages, and subjected them to dilute acid hydrolysis. The viscosity average degrees of polymerization (DPv) of the wood celluloses decreased in DPv with increasing dilute acid-hydrolysis times. However, the DPv values after 4h of acid hydrolysis differed from those of softwood bleached kraft pulp (SBKP), which showed typical patterns of LODPs. Thus, the disordered regions corresponding to LODPs that were observed for SBKP are probably not synthesized in the native wood. Instead, such disordered regions are formed secondarily or artificially during the isolation/purification and/or drying processes of plant cellulose fibers. The results of the dilute acid hydrolysis and the 2,2,6,6-tetramethylpiperidine-1-oxyl radical (TEMPO)-mediated oxidation of SBKP and softwood unbleached soda-anthraquinone pulp showed that the structures of disordered regions can be controlled via the preparation and drying conditions of wood cellulose used as starting materials.
journal_name
Int J Biol Macromoljournal_title
International journal of biological macromoleculesauthors
Funahashi R,Ono Y,Tanaka R,Yokoi M,Daido K,Inamochi T,Saito T,Horikawa Y,Isogai Adoi
10.1016/j.ijbiomac.2017.11.078subject
Has Abstractpub_date
2018-04-01 00:00:00pages
914-920eissn
0141-8130issn
1879-0003pii
S0141-8130(17)33896-5journal_volume
109pub_type
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