Abstract：
:A portable capillary electrophoresis instrument with dual capacitively coupled contactless conductivity detection (C4 D) was used to determine the inorganic ionic profiles of three pharmaceutical samples and precursors of two illicit drugs (contemporary samples of methylone and para-methoxymethamphetamine). The LODs ranged from 0.10 μmol/L to 1.25 μmol/L for the 10 selected cations, and from 0.13 μmol/L to 1.03 μmol/L for the eight selected anions. All separations were performed in less than 6 min with migration times and peak area RSD values ranging from 2 to 7%. The results demonstrate the potential of the analysis of inorganic ionic species to aid in the identification and/or differentiation of unknown tablets, and real samples found in illicit drug manufacture scenarios. From the resulting ionic fingerprint, the unknown tablets and samples can be further classified.
journal_name
J Forensic Scijournal_title
Journal of forensic sciencesauthors
Evans E,Costrino C,do Lago CL,Garcia CD,Roux C,Blanes Ldoi
10.1111/1556-4029.13175subject
Has Abstractpub_date
2016-11-01 00:00:00pages
1610-1614issue
6eissn
0022-1198issn
1556-4029journal_volume
61pub_type
杂志文章abstract：:Determining appropriate analytical thresholds (ATs) for forensic DNA analysis is critical to maximize allele detection. In this study, six methods to determine ATs for forensic DNA purposes were examined and compared. Four of the methods rely on analysis of the baseline noise of a number of negatives, while two utiliz...
journal_title：Journal of forensic sciences
pub_type： 杂志文章
doi：10.1111/1556-4029.12008
更新日期：2013-01-01 00:00:00
abstract：:Moderate to high levels of alcohol decrease brain intracellular free magnesium concentration, a factor known to be critical in brain injury. Phosphorus magnetic resonance spectroscopy was used to examine changes to brain free magnesium concentration after blunt cranial trauma in alcohol-intoxicated rats. Rats exposed ...
journal_title：Journal of forensic sciences
pub_type： 杂志文章
doi：10.1111/j.1556-4029.2012.02108.x
更新日期：2012-07-01 00:00:00
abstract：:The fortuitous recovery of material trapped within the cavity of a hollow-point bullet at autopsy was demonstrated to be of evidentiary value. Analysis of this material, as well as that from hollow-point bullets from test-firings, showed that the contents, especially if in multiple layers, could be correlated with the...
journal_title：Journal of forensic sciences
pub_type： 杂志文章
doi：
更新日期：1988-07-01 00:00:00
abstract：:A new set of multiplexed PCR primers has been applied to the analysis of human skeletal remains to determine their efficacy in analyzing degraded DNA. These primer sets, known as Miniplexes, produce shorter amplicons (50-280 base pairs (bp)) than standard short tandem repeat (STR) kits, but still utilize the 13 CODIS ...
journal_title：Journal of forensic sciences
pub_type： 杂志文章
doi：10.1111/j.1556-4029.2006.00077.x
更新日期：2006-03-01 00:00:00
abstract：:Solid-phase microextraction/gas chromatography-mass spectrometry (SPME/GC-MS) was used to characterize the volatile components associated with U.S. currency, U.S. currency inks, and Canadian currency. Compounds that can be attributed to the ink-curing process include series of straight-chain aldehydes, alkenals, acids...
journal_title：Journal of forensic sciences
pub_type： 杂志文章
doi：
更新日期：2003-07-01 00:00:00
abstract：:The full childhood triad of enuresis, firesetting, and cruelty to animals is seldom reported by patients in acute care psychiatric facilities. Two of the three elements have been reported with greater frequency and constitute useful diagnostic information. Literature on the triad has been reviewed and data from three ...
journal_title：Journal of forensic sciences
pub_type： 杂志文章
doi：
更新日期：1979-01-01 00:00:00
abstract：:Two hundred and twenty-eight consecutive medicolegal autopsies were studied as to the cause of death established by a physician, the mode of death as suggested in the police report, and findings of medical interest often discovered following autopsy. Corrections had to be made even in some cases which seemed to be obv...
journal_title：Journal of forensic sciences
pub_type： 杂志文章
doi：
更新日期：1988-03-01 00:00:00
abstract：:Maximum length measurement of the tibia has been found to be variable both in description and implementation. Historically, the literature often excludes the intercondylar eminences from the tibia in metric analysis. This paper explores the quantitative effects of inclusion or exclusion of the eminences on the maximum...
journal_title：Journal of forensic sciences
pub_type： 杂志文章
doi：10.1111/j.1556-4029.2009.01222.x
更新日期：2010-01-01 00:00:00
abstract：:Six multiplex PCR systems using single-base extension reactions to analyze 46 mitochondrial DNA (mtDNA)-coding region single nucleotide polymorphisms (SNPs) that define 42 haplogroups, that is, 24 major mtDNA haplogroups and 18 subclades, were devised. To improve the usefulness of the established systems for the analy...
journal_title：Journal of forensic sciences
pub_type： 杂志文章
doi：10.1111/1556-4029.12961
更新日期：2016-03-01 00:00:00
abstract：:Purification methods of deoxyribonucleic acid (DNA) from degraded and contaminated forensic samples were investigated for polymerase chain reaction (PCR) analysis. DNA extracted from putrefied tissue or bloodstains sometimes contained the copurified contaminant, that was identified as the porphyrin compound (hematin)....
journal_title：Journal of forensic sciences
pub_type： 杂志文章
doi：
更新日期：1993-05-01 00:00:00
abstract：:The high-performance liquid chromatographic resolution of the enantiomers of amphetamine, methamphetamine, ephedrine, and pseudoephedrine is described. The sugar isothiocyanate, 2,3,4,6-tetra-O-acetyl-beta-D-glucopyranosyl isothiocyanate (GITC), is used as a chiral derivatizing agent, with chromatographic separations ...
journal_title：Journal of forensic sciences
pub_type： 杂志文章
doi：
更新日期：1986-04-01 00:00:00
abstract：:Internal standards are commonly used for the quantitative determination of drugs of abuse and their metabolites (drug/metabolite) in biological fluids and tissues by the selective ion monitoring (SIM) gas chromatography/mass spectrometry (GC/MS) procedure. Analogs of drugs/metabolites that are labeled with three or mo...
journal_title：Journal of forensic sciences
pub_type： 杂志文章
doi：
更新日期：1995-11-01 00:00:00
abstract：:Allele frequencies for the locus D1S80 were determined in African American, Caucasian, Southeastern Hispanic, Southwestern Hispanic, and Oriental sample populations using the polymerase chain reaction and subsequent electrophoresis and silver staining of the amplified products. Due to the presence of anodal and cathod...
journal_title：Journal of forensic sciences
pub_type： 杂志文章
doi：
更新日期：1995-01-01 00:00:00
abstract：:Three new color/screening tests for flunitrazepam (Rohypnol) are reported. The two-step tests are simple, sensitive, highly specific, and effective for both cut and uncut flunitrazepam and standard over-the-counter preparations of flunitrazepam (i.e., Rohypnol tablets). ...
journal_title：Journal of forensic sciences
pub_type： 杂志文章
doi：
更新日期：1999-03-01 00:00:00
abstract：:A simple method for quantification of contrast in a fingerprint is proposed. Contrast is defined as the average difference in intensity of pixels between valleys and ridges in a fingerprint. It is quantified from a scanner-acquired image of the fingerprint using a histogram function of Adobe Photoshop. The method was ...
journal_title：Journal of forensic sciences
pub_type： 杂志文章
doi：10.1111/1556-4029.12224
更新日期：2013-09-01 00:00:00
abstract：:Deoxyribonucleic acid (DNA) samples extracted from stained pap smear, semen smear and postcoital slides were amplified by the polymerase chain reaction (PCR) and typed for the AmpliType PM and HLA DQ alpha alleles. HLA DQ alpha and PM types consistent with blood controls from the donors were obtained. Stained cells fi...
journal_title：Journal of forensic sciences
pub_type： 杂志文章
doi：
更新日期：1995-03-01 00:00:00
abstract：:Five different types of bullets, representing the major materials used in centerfire handgun and rifle ammunition, were inserted into the cranial, chest and abdominal cavities, muscle and adipose tissues of a fresh cadaver. The bullets were retrieved after the body was 90% decomposed. Observation and comparison of bef...
journal_title：Journal of forensic sciences
pub_type： 杂志文章
doi：
更新日期：1993-05-01 00:00:00
abstract：:Genetic marker analysis is a powerful tool for solving paternity-related problems when the putative father is missing. This report describes the first time this approach was employed in Chile to solve such a problem. In the case presented, the alleged father was missing as a result of the political detentions that too...
journal_title：Journal of forensic sciences
pub_type： 杂志文章
doi：
更新日期：1999-05-01 00:00:00
abstract：:The movement toward private sector involvement in our correctional services and programs is growing. Before our focus is turned completely to privatization of these services, it would be prudent to analyze the "policy impact of such change. It is evident that the diverse and incompatible policies guiding the governmen...
journal_title：Journal of forensic sciences
pub_type： 杂志文章
doi：
更新日期：1987-01-01 00:00:00
abstract：:Both among psychiatric inpatients and inmates of prisons and jails, suicide is highly prevalent with alarming rates. In many countries, there has been a call for action to prevent such deaths and to educate staff in the early recognition of suicide risk. A careful MedLine search was used to identify relevant papers de...
journal_title：Journal of forensic sciences
pub_type： 杂志文章,评审
doi：10.1111/j.1556-4029.2009.01122.x
更新日期：2009-09-01 00:00:00
abstract：:Alcohol-related amnesia--alcohol blackout--is a common claim of criminal defendants. The generally held belief is that during an alcohol blackout, other cognitive functioning is severely impaired or absent. The presentation of alcohol blackout as scientific evidence in court requires that the science meets legal relia...
journal_title：Journal of forensic sciences
pub_type： 杂志文章,评审
doi：10.1111/1556-4029.12134
更新日期：2013-07-01 00:00:00
abstract：:Electrokinetic injection (EI) is the primary method used in forensic laboratories to load amplified PCR product in capillary electrophoresis for short tandem repeat (STR) fragment separation. Because all samples subjected to capillary electrophoresis use internal lane standard (ILS), this study investigated the conseq...
journal_title：Journal of forensic sciences
pub_type： 杂志文章
doi：10.1111/1556-4029.12945
更新日期：2016-01-01 00:00:00
abstract：:The costoclavicular (rhomboid) ligament connects the first rib to the clavicle, stabilizing the pectoral girdle. It produces skeletal traits that may be tubercles, roughened impressions, shallow groove-like fossae, deep fossae, or leave no trace. A pit or depression at this site is often called a "rhomboid fossa." Whi...
journal_title：Journal of forensic sciences
pub_type： 杂志文章
doi：
更新日期：2000-01-01 00:00:00
abstract：:In this report, the authors present a case of unusual, accidental methadone intoxication in a 40-year-old man, who had inhaled methadone powder. The drug dealer was a pharmacy technician; methadone had been stolen from a pharmacy and sold as cocaine. After having inhaled methadone powder, he suffered cardiopulmonary a...
journal_title：Journal of forensic sciences
pub_type： 杂志文章
doi：10.1111/j.1556-4029.2011.01730.x
更新日期：2011-07-01 00:00:00
abstract：:We herein report the case of a 36-year-old man who died suddenly after a fight with another man. Forensic investigations included unenhanced computed tomography, postmortem angiography, autopsy, histology, neuropathology, toxicology, and biochemistry and allowed a traumatic cause of death to be excluded. An electrocar...
journal_title：Journal of forensic sciences
pub_type： 杂志文章
doi：10.1111/1556-4029.12362
更新日期：2014-05-01 00:00:00
abstract：:Timing of oviposition on a corpse is a key factor in entomologically based minimum postmortem interval (mPMI) calculations. However, there is considerable variation in nocturnal oviposition behavior of blow flies reported in the research literature. This study investigated nocturnal oviposition in central England for ...
journal_title：Journal of forensic sciences
pub_type： 杂志文章
doi：10.1111/1556-4029.12841
更新日期：2015-11-01 00:00:00
abstract：:The primary objective of this paper is to report on the successful implementation of forensic facial approximation in a real case in the forensic context. A three-dimensional (3D) facial approximation protocol of the skull was performed with free software, applying techniques in a virtual environment that have already...
journal_title：Journal of forensic sciences
pub_type：
doi：10.1111/1556-4029.14587
更新日期：2021-01-01 00:00:00
abstract：:The effect of temperature on microbial fermentation in blood was studied. Specimens of human blood from a blood bank were inoculated with Candida albicans, an organism capable of causing fermentation. A preservative was added to a portion of the inoculated specimens. These inoculated specimens, as well as uninoculated...
journal_title：Journal of forensic sciences
pub_type： 杂志文章
doi：
更新日期：1989-01-01 00:00:00
abstract：:The association between perpetration of sexual abuse and the offender's own victimization as a child has been well documented in the literature. Various researchers have examined this relationship by assessing the exclusiveness of the sexual abuser's behavior, the gender of his victims and the gender of his own childh...
journal_title：Journal of forensic sciences
pub_type： 杂志文章
doi：
更新日期：1993-03-01 00:00:00
abstract：:Respiratory pathogens have been detected in forensic investigations using multiple techniques; however, no study has examined the use of automated, nested, multiplex polymerase chain reaction (ANM-PCR), commonly used in living patients, in the forensic setting. This retrospective study assessed the utility of ANM-PCR ...
journal_title：Journal of forensic sciences
pub_type： 杂志文章
doi：10.1111/1556-4029.13415
更新日期：2017-09-01 00:00:00
