Surfactant-free solid dispersion of fat-soluble flavour in an amorphous sugar matrix.

Abstract:

:A solid dispersion technique to homogeneously disperse hydrophobic ingredients in a water-soluble solid without using surfactant was examined as follows: first, freeze-dried amorphous sugar was dissolved in an organic medium that contained a soluble model hydrophobic component. Second, the mixed solution of sugar and the model hydrophobic component was vacuum dried into a solid (solid dispersion). Methanol and six fat-soluble flavours, including cinnamaldehyde, were used as organic media and model hydrophobic components. The retention of flavours in the solid dispersion during drying and storage under vacuum was evaluated. The amorphised disaccharides dissolved in methanol up to 100mg/mL, even temporarily (20s to 10 days) and could be solidified without any evidence of crystallisation and segregation from flavour. The solid dispersion, prepared using α-maltose usually showed 65-95% flavour retention during drying (and storage for cinnamaldehyde), whereas ⩾ 50% of the flavour was lost when the flavour was O/W emulsified with a surfactant and then freeze-dried with sugar.

journal_name

Food Chem

journal_title

Food chemistry

authors

Satoh T,Hidaka F,Miyake K,Yoshiyama N,Takeda K,Matsuura T,Imanaka H,Ishida N,Imamura K

doi

10.1016/j.foodchem.2015.11.097

subject

Has Abstract

pub_date

2016-04-15 00:00:00

pages

1136-42

eissn

0308-8146

issn

1873-7072

pii

S0308-8146(15)30242-9

journal_volume

197 Pt B

pub_type

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